C₂₇H₃₂IN₅O₄

Base Information

Chemical Name:C₂₇H₃₂IN₅O₄
CAS No.:1314136-69-0
Molecular Formula:C₂₇H₃₂IN₅O₄
Molecular Weight:617.487
Hs Code.:

C<sub>27</sub>H<sub>32</sub>IN<sub>5</sub>O<sub>4</sub>

Synonyms:C₂₇H₃₂IN₅O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₂IN₅O₄

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Technology Process of C₂₇H₃₂IN₅O₄

There total 8 articles about C₂₇H₃₂IN₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1314137-13-7
C₂₇H₃₂IN₅O₄

: 1314136-69-0
C₂₇H₃₂IN₅O₄

Guidance literature:: With copper; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 100 ℃; for 0.166667h; Copper flow reactor;
DOI:10.1021/ol201567s

Reference yield:

: 1314137-07-9
C₂₄H₃₂N₂O₅

: 1314136-69-0
C₂₇H₃₂IN₅O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrabutyl ammonium fluoride; sodium hydride / tetrahydrofuran / 20 °C

1.2: 20 °C

2.1: hydrogenchloride / 1,4-dioxane / 20 °C

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: copper(l) iodide; N-iodomorpholine-hydrogen iodide / tetrahydrofuran / 20 °C / Molecular sieve

5.1: copper; N-ethyl-N,N-diisopropylamine / acetonitrile / 0.17 h / 100 °C / Copper flow reactor

With hydrogenchloride; copper(l) iodide; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-iodomorpholine-hydrogen iodide; copper; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; acetonitrile;
DOI:10.1021/ol201567s

Reference yield:

: C₂₂H₂₆N₂O₃

: 1314136-69-0
C₂₇H₃₂IN₅O₄

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: copper(l) iodide; N-iodomorpholine-hydrogen iodide / tetrahydrofuran / 20 °C / Molecular sieve

3: copper; N-ethyl-N,N-diisopropylamine / acetonitrile / 0.17 h / 100 °C / Copper flow reactor

With copper(l) iodide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-iodomorpholine-hydrogen iodide; copper; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ol201567s