phorbol 12,13-di(allyl terephthalate)-20-trityl

Base Information

Chemical Name:phorbol 12,13-di(allyl terephthalate)-20-trityl
CAS No.:561063-38-5
Molecular Formula:C₆₁H₅₈O₁₂
Molecular Weight:983.124
Hs Code.:

Synonyms:phorbol 12,13-di(allyl terephthalate)-20-trityl

Suppliers and Price of phorbol 12,13-di(allyl terephthalate)-20-trityl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phorbol 12,13-di(allyl terephthalate)-20-trityl

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phorbol 12,13-di(allyl terephthalate)-20-trityl

There total 1 articles about phorbol 12,13-di(allyl terephthalate)-20-trityl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 82400-03-1
phorbol-20-trityl ether

: 142650-66-6
4-(allyloxycarbonyl)benzoic acid

: 561063-38-5
phorbol 12,13-di(allyl terephthalate)-20-trityl

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at -78 - 20 ℃;
DOI:10.1021/jo030029w

Reference yield: 35.0%

: 561063-38-5
phorbol 12,13-di(allyl terephthalate)-20-trityl

: 561063-39-6
phorbol 12,13-diterephthalate-20-trityl

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; at 20 ℃; for 96h;
DOI:10.1021/jo030029w

Reference yield:

: 561063-38-5
phorbol 12,13-di(allyl terephthalate)-20-trityl

: phorbol 12,13-diterephthalate

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / morpholine; Pd(PPh₃)4 / CH₂Cl₂ / 96 h / 20 °C

2: 69 percent / TFA; anisole / CH₂Cl₂ / 2 h / 0 °C

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; methoxybenzene; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo030029w