4-((2-dimethylaminophenyl)methyl)-1,1,3-trimethyl-2,3-dihydroperimidinium chloride

Base Information

Chemical Name:4-((2-dimethylaminophenyl)methyl)-1,1,3-trimethyl-2,3-dihydroperimidinium chloride
CAS No.:1290176-02-1
Molecular Formula:C₂₃H₂₈N₃*Cl
Molecular Weight:381.948
Hs Code.:

Synonyms:4-((2-dimethylaminophenyl)methyl)-1,1,3-trimethyl-2,3-dihydroperimidinium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-((2-dimethylaminophenyl)methyl)-1,1,3-trimethyl-2,3-dihydroperimidinium chloride

Chemical Property:

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Technology Process of 4-((2-dimethylaminophenyl)methyl)-1,1,3-trimethyl-2,3-dihydroperimidinium chloride

There total 2 articles about 4-((2-dimethylaminophenyl)methyl)-1,1,3-trimethyl-2,3-dihydroperimidinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1290176-01-0
[1,8-bis(dimethylamino)naphth-2-yl](2'-dimethylaminophenyl)methanol

: 1290176-02-1
4-((2-dimethylaminophenyl)methyl)-1,1,3-trimethyl-2,3-dihydroperimidinium chloride

Guidance literature:: With hydrogenchloride; In water; for 3h; Reflux;
DOI:10.1039/c0ob00899k

Reference yield:

: 579-72-6
2-(dimethylamino)benzaldehyde

: 206761-13-9
{1,8-bis(dimethylamino)naphthalene-2-yl} bromide

: 1290176-02-1
4-((2-dimethylaminophenyl)methyl)-1,1,3-trimethyl-2,3-dihydroperimidinium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -15 °C

1.2: -15 °C

2.1: hydrogenchloride / water / 3 h / Reflux

With hydrogenchloride; n-butyllithium; In diethyl ether; hexane; water;
DOI:10.1039/c0ob00899k