methyl 6-deoxy-6-(diethylphospate)-2,3,4-tri-O-benzyl-α-D-mannopyranozide

Base Information

Chemical Name:methyl 6-deoxy-6-(diethylphospate)-2,3,4-tri-O-benzyl-α-D-mannopyranozide
CAS No.:1304043-53-5
Molecular Formula:C₃₂H₄₁O₉P
Molecular Weight:600.646
Hs Code.:

Synonyms:methyl 6-deoxy-6-(diethylphospate)-2,3,4-tri-O-benzyl-α-D-mannopyranozide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-deoxy-6-(diethylphospate)-2,3,4-tri-O-benzyl-α-D-mannopyranozide

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Technology Process of methyl 6-deoxy-6-(diethylphospate)-2,3,4-tri-O-benzyl-α-D-mannopyranozide

There total 5 articles about methyl 6-deoxy-6-(diethylphospate)-2,3,4-tri-O-benzyl-α-D-mannopyranozide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₄₁O₈P

: 1304043-53-5
methyl 6-deoxy-6-(diethylphospate)-2,3,4-tri-O-benzyl-α-D-mannopyranozide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 20 ℃; for 0.333333h;

Reference yield:

: 34212-64-1,641635-63-4
methyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside

: 1304043-53-5
methyl 6-deoxy-6-(diethylphospate)-2,3,4-tri-O-benzyl-α-D-mannopyranozide

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h / -78 - 20 °C

With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 617-04-9
(2R,3S,4S,5S,6S)-2-(hydroxymethyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triol

: 1304043-53-5
methyl 6-deoxy-6-(diethylphospate)-2,3,4-tri-O-benzyl-α-D-mannopyranozide

Guidance literature:: Multi-step reaction with 5 steps

1: dmap; pyridine / 1.5 h

2: potassium hydroxide / 1 h / 80 °C

3: water; ammonium cerium (IV) nitrate / acetonitrile / 60 °C

4: 1H-tetrazole / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h / -78 - 20 °C

With pyridine; 1H-tetrazole; dmap; ammonium cerium (IV) nitrate; water; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In tetrahydrofuran; dichloromethane; acetonitrile;