2'-C-methylguanosine 5'-(O-phenyl-N-(S)-1-(neopentoxycarbonyl)ethyl)thiophosphoramidate

Base Information

Chemical Name:2'-C-methylguanosine 5'-(O-phenyl-N-(S)-1-(neopentoxycarbonyl)ethyl)thiophosphoramidate
CAS No.:1365634-84-9
Molecular Formula:C₂₅H₃₅N₆O₈PS
Molecular Weight:610.628
Hs Code.:

Synonyms:2'-C-methylguanosine 5'-(O-phenyl-N-(S)-1-(neopentoxycarbonyl)ethyl)thiophosphoramidate

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Chemical Property of 2'-C-methylguanosine 5'-(O-phenyl-N-(S)-1-(neopentoxycarbonyl)ethyl)thiophosphoramidate

Chemical Property:

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Technology Process of 2'-C-methylguanosine 5'-(O-phenyl-N-(S)-1-(neopentoxycarbonyl)ethyl)thiophosphoramidate

There total 3 articles about 2'-C-methylguanosine 5'-(O-phenyl-N-(S)-1-(neopentoxycarbonyl)ethyl)thiophosphoramidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₅H₅₁N₆O₉PS

: 1365634-84-9
2'-C-methylguanosine 5'-(O-phenyl-N-(S)-1-(neopentoxycarbonyl)ethyl)thiophosphoramidate

Guidance literature:: With formic acid; In water; at 20 ℃;

Reference yield:

: 1365634-83-8
C₃₃H₃₃N₅O₇

: 1365634-84-9
2'-C-methylguanosine 5'-(O-phenyl-N-(S)-1-(neopentoxycarbonyl)ethyl)thiophosphoramidate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 h / 82 °C

2: formic acid / water / 20 °C

With formic acid; N-ethyl-N,N-diisopropylamine; In water; acetonitrile;

Reference yield:

: 1036915-16-8
C₁₃H₁₇N₅O₆

: 1365634-84-9
2'-C-methylguanosine 5'-(O-phenyl-N-(S)-1-(neopentoxycarbonyl)ethyl)thiophosphoramidate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; tert-butyldimethylsilyl chloride; pyridine / 25 °C

1.2: 3 h / 50 °C

1.3: 20 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 h / 82 °C

3.1: formic acid / water / 20 °C

With pyridine; dmap; formic acid; tert-butyldimethylsilyl chloride; N-ethyl-N,N-diisopropylamine; In water; acetonitrile;