4-phenyl-thiobutyric acid amide

Base Information

• Chemical Name: 4-phenyl-thiobutyric acid amide
• CAS No.: 177665-17-7
• Molecular Formula: C₁₀H₁₃NS
• Molecular Weight: 179.286

Synonyms:4-phenyl-thiobutyric acid amide

Chemical Property of 4-phenyl-thiobutyric acid amide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

4-phenylbutanethioamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-phenyl-thiobutyric acid amide

There total 2 articles about 4-phenyl-thiobutyric acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Lawessons reagent (19172-47-5,94367-93-8) + 4-phenylbutyramide (1199-98-0) → 4-phenyl-thiobutyric acid amide (177665-17-7)

Guidance literature:

With acetic acid; In hexane; toluene;

Reference yield:

4-phenylbutyronitrile (2046-18-6) → 4-phenyl-thiobutyric acid amide (177665-17-7)

Guidance literature:

With hydrogen sulfide; sodium ethanolate; at 60.6 ℃; under 1330 Torr;

Reference yield:

4-phenyl-thiobutyric acid amide (177665-17-7) + 1-(4-fluorophenyl)-2-(4-methylthiophenyl)-2-bromoethanone (71006-38-7) → 4-(4-fluorophenyl)-5-(4-methylthiophenyl)-2-(3-phenylpropyl)thiazole (177561-41-0)

Guidance literature:

In acetonitrile; Heating;

DOI:10.1016/S0960-894X(99)00158-4

upstream raw materials:

4-phenylbutyronitrile

Lawessons reagent

4-phenylbutyramide

Downstream raw materials:

4-(4-fluorophenyl)-5-(4-methylthiophenyl)-2-(3-phenylpropyl)thiazole

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