2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allose ethylene acetal

Base Information

Chemical Name:2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allose ethylene acetal
CAS No.:294664-38-3
Molecular Formula:C₂₉H₂₇NO₈
Molecular Weight:517.535
Hs Code.:

Synonyms:2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allose ethylene acetal

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Chemical Property of 2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allose ethylene acetal

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Technology Process of 2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allose ethylene acetal

There total 6 articles about 2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allose ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 582-25-2
Potassium benzoate

: 294664-38-3
2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allose ethylene acetal

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / dimethylformamide / 48 h / 100 °C

2: 77 percent / NaN₃ / dimethylsulfoxide / 47 h / 115 - 120 °C

3: H₂ / 10 percent Pd/C / ethanol; CHCl₃ / 120 h / 20 °C

4: 4.67 g / pyridine / 96 h / 20 °C

With pyridine; sodium azide; hydrogen; palladium on activated charcoal; In ethanol; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)01126-7

Reference yield:

: 157506-35-9
2,5-anhydro-3,6-di-O-methanesulfonyl-D-glucose ethylene acetal

: 294664-38-3
2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allose ethylene acetal

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / Ag₂O / diethyl ether / 22 h / Heating

2: 83 percent / dimethylformamide / 48 h / 100 °C

3: 77 percent / NaN₃ / dimethylsulfoxide / 47 h / 115 - 120 °C

4: H₂ / 10 percent Pd/C / ethanol; CHCl₃ / 120 h / 20 °C

5: 4.67 g / pyridine / 96 h / 20 °C

With pyridine; sodium azide; hydrogen; silver(l) oxide; palladium on activated charcoal; In diethyl ether; ethanol; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)01126-7

Reference yield:

: 228398-97-8
2,5-anhydro-4-O-benzyl-3,6-di-O-methanesulfonyl-D-glucose ethylene acetal

: 294664-38-3
2,5-anhydro-3-benzamido-4,6-di-O-benzoyl-3-deoxy-D-allose ethylene acetal

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / dimethylformamide / 48 h / 100 °C

2: 77 percent / NaN₃ / dimethylsulfoxide / 47 h / 115 - 120 °C

3: H₂ / 10 percent Pd/C / ethanol; CHCl₃ / 120 h / 20 °C

4: 4.67 g / pyridine / 96 h / 20 °C

With pyridine; sodium azide; hydrogen; palladium on activated charcoal; In ethanol; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)01126-7