(Endo)-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane hydrochloride

Base Information

• Chemical Name: (Endo)-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane hydrochloride
• CAS No.: 1182356-81-5
• Molecular Formula: C₁₅H₂₀FNO*ClH
• Molecular Weight: 285.789

Synonyms:(Endo)-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane hydrochloride

Chemical Property of (Endo)-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane hydrochloride

Chemical Property:

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Technology Process of (Endo)-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane hydrochloride

There total 1 articles about (Endo)-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Endo)-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane-8-carboxylic acid tert-butyl ester (1182356-80-4) → (Endo)-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane hydrochloride (1182356-81-5)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃; for 2h;

Reference yield:

(Endo)-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane hydrochloride (1182356-81-5) + trans-(2-bromomethylcyclopropylmethoxy)-tert-butyldiphenylsilane → (endo)-8-[trans-2-(tert-butyldiphenylsilanyloxymethyl)cyclopropylmethyl]-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;

Reference yield:

(Endo)-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane hydrochloride (1182356-81-5) + 4-ethyl-2-(R)-1-oxiranylmethyl-2,4-dihydro[1,2,4]triazol-3-one (1182358-39-9) → (endo)-4-ethyl-2-{(S)-3-[3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]oct-8-yl]-2-hydroxy-propyl}-2,4-dihydro[1,2,4]triazol-3-one (1182354-12-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 24h;

upstream raw materials:

(Endo)-3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]octane-8-carboxylic acid tert-butyl ester

Downstream raw materials:

(endo)-4-ethyl-2-{(S)-3-[3-(2-fluoro-6-methylbenzyloxy)-8-azabicyclo[3.2.1]oct-8-yl]-2-hydroxy-propyl}-2,4-dihydro[1,2,4]triazol-3-one

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