(3-(1-(3,5-dichlorophenyl)-3-methyl-6-oxo-1,6-dihydropyridazin-4-yl)-phenyl)ethanesulfonamide

Base Information

Chemical Name:(3-(1-(3,5-dichlorophenyl)-3-methyl-6-oxo-1,6-dihydropyridazin-4-yl)-phenyl)ethanesulfonamide
CAS No.:1402614-35-0
Molecular Formula:C₁₉H₁₇Cl₂N₃O₃S
Molecular Weight:438.334
Hs Code.:

Synonyms:(3-(1-(3,5-dichlorophenyl)-3-methyl-6-oxo-1,6-dihydropyridazin-4-yl)-phenyl)ethanesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-(1-(3,5-dichlorophenyl)-3-methyl-6-oxo-1,6-dihydropyridazin-4-yl)-phenyl)ethanesulfonamide

Chemical Property:

Purity/Quality:

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Technology Process of (3-(1-(3,5-dichlorophenyl)-3-methyl-6-oxo-1,6-dihydropyridazin-4-yl)-phenyl)ethanesulfonamide

There total 8 articles about (3-(1-(3,5-dichlorophenyl)-3-methyl-6-oxo-1,6-dihydropyridazin-4-yl)-phenyl)ethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402615-04-6
C₁₃H₁₅N₃O₃S

: 67492-50-6
(3,5-dichlorophenyl)boronic acid

: 1402614-35-0
(3-(1-(3,5-dichlorophenyl)-3-methyl-6-oxo-1,6-dihydropyridazin-4-yl)-phenyl)ethanesulfonamide

Guidance literature:: With copper diacetate; triethylamine; In dichloromethane; at 20 ℃; Molecular sieve;
DOI:10.1016/j.bmcl.2013.04.065

Reference yield:

: 1402614-94-1
C₁₁H₁₁N₃O₃

: 1402614-35-0
(3-(1-(3,5-dichlorophenyl)-3-methyl-6-oxo-1,6-dihydropyridazin-4-yl)-phenyl)ethanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: selenium(IV) oxide; acetic acid / 3 h / 100 °C

2: iron; hydrogenchloride / ethanol; water / 2 h / Reflux

3: pyridine / 2 h / 50 °C

4: copper diacetate; triethylamine / dichloromethane / 20 °C / Molecular sieve

With pyridine; hydrogenchloride; selenium(IV) oxide; copper diacetate; iron; acetic acid; triethylamine; In ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.04.065

Reference yield:

: 1402614-89-4
C₁₁H₁₁NO₅

: 1402614-35-0
(3-(1-(3,5-dichlorophenyl)-3-methyl-6-oxo-1,6-dihydropyridazin-4-yl)-phenyl)ethanesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: hydrazine / ethanol / 3 h / Reflux

2: selenium(IV) oxide; acetic acid / 3 h / 100 °C

3: iron; hydrogenchloride / ethanol; water / 2 h / Reflux

4: pyridine / 2 h / 50 °C

5: copper diacetate; triethylamine / dichloromethane / 20 °C / Molecular sieve

With pyridine; hydrogenchloride; selenium(IV) oxide; copper diacetate; iron; acetic acid; triethylamine; hydrazine; In ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.04.065