(1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-bis-(2-methoxy-ethoxymethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid trimethyl ester

Base Information

Chemical Name:(1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-bis-(2-methoxy-ethoxymethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid trimethyl ester
CAS No.:170156-59-9
Molecular Formula:C₄₆H₆₈O₁₈
Molecular Weight:909.035
Hs Code.:

(1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-bis-(2-methoxy-ethoxymethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid trimethyl ester

Synonyms:(1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-bis-(2-methoxy-ethoxymethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid trimethyl ester

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Chemical Property of (1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-bis-(2-methoxy-ethoxymethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid trimethyl ester

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Technology Process of (1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-bis-(2-methoxy-ethoxymethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid trimethyl ester

There total 3 articles about (1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-bis-(2-methoxy-ethoxymethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid trimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 147506-51-2
(1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4-hydroxy-7-(2-methoxy-ethoxymethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid trimethyl ester

: 170156-59-9
(1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-bis-(2-methoxy-ethoxymethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid trimethyl ester

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; paraffin; at 20 ℃; for 96h;

Reference yield:

: 138682-84-5,144786-97-0,146075-86-7,148152-80-1,149656-40-6,142561-96-4
zaragozic acid A

: 170156-59-9
(1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-bis-(2-methoxy-ethoxymethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid trimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / methanol; diethyl ether / 15 h / 20 °C

2: 75 percent / diisopropylethylamine / 1,2-dichloro-ethane / 20 h / Heating

3: 90 percent / NaH / dimethylformamide; paraffin / 96 h / 20 °C

With sodium hydride; N-ethyl-N,N-diisopropylamine; In methanol; diethyl ether; 1,2-dichloro-ethane; N,N-dimethyl-formamide; paraffin;

Reference yield:

: 142561-97-5
zaragozic acid A trimethyl ester

: 170156-59-9
(1S,3S,4S,5R,6R,7R)-1-((4S,5R)-4-Acetoxy-5-methyl-3-methylene-6-phenyl-hexyl)-6-((E)-(4S,6S)-4,6-dimethyl-oct-2-enoyloxy)-4,7-bis-(2-methoxy-ethoxymethoxy)-2,8-dioxa-bicyclo[3.2.1]octane-3,4,5-tricarboxylic acid trimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / diisopropylethylamine / 1,2-dichloro-ethane / 20 h / Heating

2: 90 percent / NaH / dimethylformamide; paraffin / 96 h / 20 °C

With sodium hydride; N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; paraffin;