phenyl 2^I,3^I,6^I,2^II,3^II,6^II,2^III,3^III,6^III,2^IV,3^IV,6^IV,2^V,3^V,6^V,2^VI,3^VI,6^VI-octadeca-O-benzyl-1^I-thio-β-maltohexaoside

Base Information

• Chemical Name: phenyl 2^I,3^I,6^I,2^II,3^II,6^II,2^III,3^III,6^III,2^IV,3^IV,6^IV,2^V,3^V,6^V,2^VI,3^VI,6^VI-octadeca-O-benzyl-1^I-thio-β-maltohexaoside
• CAS No.: 134241-82-0
• Molecular Formula: C₁₆₈H₁₇₄O₃₀S
• Molecular Weight: 2705.28

Synonyms:phenyl 2^I,3^I,6^I,2^II,3^II,6^II,2^III,3^III,6^III,2^IV,3^IV,6^IV,2^V,3^V,6^V,2^VI,3^VI,6^VI-octadeca-O-benzyl-1^I-thio-β-maltohexaoside

Chemical Property of phenyl 2^I,3^I,6^I,2^II,3^II,6^II,2^III,3^III,6^III,2^IV,3^IV,6^IV,2^V,3^V,6^V,2^VI,3^VI,6^VI-octadeca-O-benzyl-1^I-thio-β-maltohexaoside

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Technology Process of phenyl 2^I,3^I,6^I,2^II,3^II,6^II,2^III,3^III,6^III,2^IV,3^IV,6^IV,2^V,3^V,6^V,2^VI,3^VI,6^VI-octadeca-O-benzyl-1^I-thio-β-maltohexaoside

There total 1 articles about phenyl 2^I,3^I,6^I,2^II,3^II,6^II,2^III,3^III,6^III,2^IV,3^IV,6^IV,2^V,3^V,6^V,2^VI,3^VI,6^VI-octadeca-O-benzyl-1^I-thio-β-maltohexaoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

phenyl 2I,3I,6I,2II,3II,6II, 2III,3III,6III,2IV,3IV,6IV,2V,3V,6V,2VI,3VI-heptadeca-O-benzyl-4VI,6VI-O-benzylidene-1I-thio-β-maltohexaoside (134237-73-3,149342-85-8) → phenyl 2I,3I,6I,2II,3II,6II,2III,3III,6III,2IV,3IV,6IV,2V,3V,6V,2VI,3VI,6VI-octadeca-O-benzyl-1I-thio-β-maltohexaoside (134241-82-0)

Guidance literature:

With aluminium trichloride; acetonitrile - borane (1/1); 4 A molecular sieve; In tetrahydrofuran; for 48h; Ambient temperature;

DOI:10.1039/c39910000289

Reference yield: 18.0%

phenyl 2I,3I,6I,2II,3II,6II,2III,3III,6III,2IV,3IV,6IV,2V,3V,6V,2VI,3VI,6VI-octadeca-O-benzyl-1I-thio-β-maltohexaoside (134241-82-0) + methyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-(p-methoxybenzyl)-1-thio-α,β-glucopyranoside → phenyl 6VII-O-acetyl-2VII-azido-2I,3I,6I,2II,3II,6II,2III,3III,6III,2IV,3IV,6IV,2V,3V,6V,2VI,3VI,6VI,3VII-nonadeca-O-benzyl-2VII-deoxy-4VII-O-(p-methoxybenzyl)-1I-thio-β-maltoheptaoside + hexakis-(2,3,6-tri-O-benzyl)-α-cyclodextrin (110237-97-3,123930-57-4,150520-16-4)

Guidance literature:

With methyl trifluoromethanesulfonate; In diethyl ether; at 0 ℃;

upstream raw materials:

phenyl 2^I,3^I,6^I,2^II,3^II,6^II, 2^III,3^III,6^III,2^IV,3^IV,6^IV,2^V,3^V,6^V,2^VI,3^VI-heptadeca-O-benzyl-4^VI,6^VI-O-benzylidene-1^I-thio-β-maltohexaoside

Downstream raw materials:

hexakis-(2,3,6-tri-O-benzyl)-α-cyclodextrin

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