6-[(2,6-dimethoxyphenoxy)methyl]-5-methyl-2-(2-nitrophenyl)sulfonyl-2,3-dihydro-[1H]-2-benzazepine

Base Information

• Chemical Name: 6-[(2,6-dimethoxyphenoxy)methyl]-5-methyl-2-(2-nitrophenyl)sulfonyl-2,3-dihydro-[1H]-2-benzazepine
• CAS No.: 1043870-71-8
• Molecular Formula: C₂₆H₂₆N₂O₇S
• Molecular Weight: 510.568

Synonyms:6-[(2,6-dimethoxyphenoxy)methyl]-5-methyl-2-(2-nitrophenyl)sulfonyl-2,3-dihydro-[1H]-2-benzazepine

Chemical Property of 6-[(2,6-dimethoxyphenoxy)methyl]-5-methyl-2-(2-nitrophenyl)sulfonyl-2,3-dihydro-[1H]-2-benzazepine

Chemical Property:

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Technology Process of 6-[(2,6-dimethoxyphenoxy)methyl]-5-methyl-2-(2-nitrophenyl)sulfonyl-2,3-dihydro-[1H]-2-benzazepine

There total 1 articles about 6-[(2,6-dimethoxyphenoxy)methyl]-5-methyl-2-(2-nitrophenyl)sulfonyl-2,3-dihydro-[1H]-2-benzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(Z)-3-[2-hydroxymethyl-6-(2,6-dimethoxyphenoxymethyl)phenyl]but-2-enyl 2-nitrobenzenesulfonamide (1043870-83-2) → 6-[(2,6-dimethoxyphenoxy)methyl]-5-methyl-2-(2-nitrophenyl)sulfonyl-2,3-dihydro-[1H]-2-benzazepine (1043870-71-8)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1039/b801208c

Reference yield: 100.0%

6-[(2,6-dimethoxyphenoxy)methyl]-5-methyl-2-(2-nitrophenyl)sulfonyl-2,3-dihydro-[1H]-2-benzazepine (1043870-71-8) → 6-[(2,6-dimethoxyphenoxy)methyl]-5-methyl-2,3-dihydro-[1H]-2-benzazepine (1043870-93-4)

Guidance literature:

With potassium carbonate; thiophenol; In acetonitrile; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1039/b801208c

upstream raw materials:

(Z)-3-[2-hydroxymethyl-6-(2,6-dimethoxyphenoxymethyl)phenyl]but-2-enyl 2-nitrobenzenesulfonamide

Downstream raw materials:

6-[(2,6-dimethoxyphenoxy)methyl]-5-methyl-2,3-dihydro-[1H]-2-benzazepine

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