5-(3-benzyloxypropyl)-3,7-methano-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-13-on

Base Information

Chemical Name:5-(3-benzyloxypropyl)-3,7-methano-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-13-on
CAS No.:116556-63-9
Molecular Formula:C₂₅H₂₈N₂O₂
Molecular Weight:388.51
Hs Code.:

Synonyms:5-(3-benzyloxypropyl)-3,7-methano-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-13-on

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Chemical Property of 5-(3-benzyloxypropyl)-3,7-methano-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-13-on

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Technology Process of 5-(3-benzyloxypropyl)-3,7-methano-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-13-on

There total 10 articles about 5-(3-benzyloxypropyl)-3,7-methano-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-13-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 116527-84-5
9-(3-Benzyloxy-propyl)-5,8,9,10,11,12-hexahydro-6H-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester

: 116556-63-9
5-(3-benzyloxypropyl)-3,7-methano-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-13-on

: 116527-96-9
5-(3-hydroxypropyl)-3,7-methano-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-13-on

Guidance literature:: With palladium on activated charcoal; hydrogen; In ethyl acetate; at 30 - 35 ℃; for 24h;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-78-7,116556-53-7
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol-3-on

: 116556-63-9
5-(3-benzyloxypropyl)-3,7-methano-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-13-on

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / Lithium aluminium hydride / tetrahydrofuran / 1 h / Heating

2: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

3: 68 percent / HCl / CH₂Cl₂ / 2 h / Ambient temperature

4: 95 percent / water, sodium hydroxide / ethanol / 1.5 h / Heating

5: 30 percent / H₂, Pd/C / ethyl acetate / 24 h / 30 - 35 °C

With hydrogenchloride; sodium hydroxide; palladium on activated charcoal; lithium aluminium tetrahydride; water; hydrogen; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-79-8,116527-80-1
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol

: 116556-63-9
5-(3-benzyloxypropyl)-3,7-methano-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-13-on

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

2: 68 percent / HCl / CH₂Cl₂ / 2 h / Ambient temperature

3: 95 percent / water, sodium hydroxide / ethanol / 1.5 h / Heating

4: 30 percent / H₂, Pd/C / ethyl acetate / 24 h / 30 - 35 °C

With hydrogenchloride; sodium hydroxide; palladium on activated charcoal; water; hydrogen; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(01)86862-9