{1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-phenyl-amine

Base Information

• Chemical Name: {1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-phenyl-amine
• CAS No.: 1062680-29-8
• Molecular Formula: C₃₆H₄₁NO₃Si
• Molecular Weight: 563.812

Synonyms:{1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-phenyl-amine

Chemical Property of {1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-phenyl-amine

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Technology Process of {1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-phenyl-amine

There total 1 articles about {1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-phenyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

3',4'-dimethoxy-6'-(tert-butyldimethylsilyloxymethyl)[1,1'-biphenyl]-2-carbaldehyde (878198-89-1) + phenylacetylene (536-74-3) + aniline (62-53-3) → {1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-phenyl-amine (1062680-29-8)

Guidance literature:

With copper(I) bromide; at 90 ℃; for 0.333333h; microwave irradiation;

DOI:10.1021/jo801290j

Reference yield: 96.0%

{1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-phenyl-amine (1062680-29-8) + trifluoroacetic anhydride (407-25-0) → N-{1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-2,2,2-trifluoro-N-phenylacetamide (1062680-53-8)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jo801290j

Reference yield: 75.0%

{1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-phenyl-amine (1062680-29-8) + acetic anhydride (108-24-7) → N-{1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-N-phenylacetamide (1062680-41-4)

Guidance literature:

In acetonitrile; at 150 ℃; for 0.5h; microwave irradiation;

DOI:10.1021/jo801290j

upstream raw materials:

3',4'-dimethoxy-6'-(tert-butyldimethylsilyloxymethyl)[1,1'-biphenyl]-2-carbaldehyde

phenylacetylene

aniline

Downstream raw materials:

N-{1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-N-phenylacetamide

N-{1-[2'-(tert-butyldimethylsilanyloxymethyl)-4',5'-dimethoxy-biphenyl-2-yl]-3-phenylprop-2-ynyl}-2,2,2-trifluoro-N-phenylacetamide

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