(S,S)-2,2-dimethyl-α,α,α',α'-tetraphenyldioxolane-4,5-dimethanol phosphorochloridite

Base Information

Chemical Name:(S,S)-2,2-dimethyl-α,α,α',α'-tetraphenyldioxolane-4,5-dimethanol phosphorochloridite
CAS No.:945668-51-9
Molecular Formula:C₃₁H₂₈ClO₄P
Molecular Weight:530.988
Hs Code.:

Synonyms:(S,S)-2,2-dimethyl-α,α,α',α'-tetraphenyldioxolane-4,5-dimethanol phosphorochloridite

Suppliers and Price of (S,S)-2,2-dimethyl-α,α,α',α'-tetraphenyldioxolane-4,5-dimethanol phosphorochloridite

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S,S)-2,2-dimethyl-α,α,α',α'-tetraphenyldioxolane-4,5-dimethanol phosphorochloridite

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S,S)-2,2-dimethyl-α,α,α',α'-tetraphenyldioxolane-4,5-dimethanol phosphorochloridite

There total 2 articles about (S,S)-2,2-dimethyl-α,α,α',α'-tetraphenyldioxolane-4,5-dimethanol phosphorochloridite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 93222-42-5,93379-48-7,93379-49-8,118139-82-5,126639-52-9,37031-30-4
(S,S)-taddol

: 945668-51-9
(S,S)-2,2-dimethyl-α,α,α',α'-tetraphenyldioxolane-4,5-dimethanol phosphorochloridite

Guidance literature:: With triethylamine; phosphorus trichloride; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/om100236v

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 945668-51-9
(S,S)-2,2-dimethyl-α,α,α',α'-tetraphenyldioxolane-4,5-dimethanol phosphorochloridite

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; magnesium / tetrahydrofuran / Reflux

2: phosphorus trichloride; triethylamine / tetrahydrofuran

With iodine; magnesium; triethylamine; phosphorus trichloride; In tetrahydrofuran;
DOI:10.1021/jacs.7b09947