6-acetyl-5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-6-chloro-2-cyclohexenone

Base Information

Chemical Name:6-acetyl-5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-6-chloro-2-cyclohexenone
CAS No.:76678-74-5
Molecular Formula:C₂₄H₂₃ClO₄
Molecular Weight:410.897
Hs Code.:

Synonyms:6-acetyl-5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-6-chloro-2-cyclohexenone

Suppliers and Price of 6-acetyl-5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-6-chloro-2-cyclohexenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-acetyl-5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-6-chloro-2-cyclohexenone

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Technology Process of 6-acetyl-5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-6-chloro-2-cyclohexenone

There total 6 articles about 6-acetyl-5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-6-chloro-2-cyclohexenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.5%

: 62096-12-2
6-acetyl-5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-2-cyclohexenone

: 76678-74-5
6-acetyl-5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-6-chloro-2-cyclohexenone

Guidance literature:: With lithium chloride; In N,N-dimethyl-formamide; at 80 ℃; for 3h;

Reference yield:

: 62096-05-3
3-<5-(3-benzyloxy-4-methoxyphenyl)-2.4-pentadienoyl>-4-hydroxy-6-methyl-2H-2-pyranone

: 76678-74-5
6-acetyl-5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-6-chloro-2-cyclohexenone

Guidance literature:: Multi-step reaction with 4 steps

1: 68.8 percent / toluene / 1.) heating, 0.5 min; 2.) RT

2: 1.) acetic acid; 2.) AlCl₃, LiAlH₄ / 1.) H₂O, ethanol, reflux, overnight; 2.) THF, 0 deg C, overnight

3: 78.7 percent / DCC, H₃PO₄ / dimethylsulfoxide / 60 °C

4: 95.5 percent / CuCl₂*2H₂O, LiCl / dimethylformamide / 3 h / 80 °C

With lithium aluminium tetrahydride; aluminium trichloride; phosphoric acid; acetic acid; dicyclohexyl-carbodiimide; lithium chloride; In dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 62096-10-0
5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-6-(1-hydroxyethyl)-2-cyclohexenone

: 76678-74-5
6-acetyl-5-<2-(3-benzyloxy-4-methoxyphenyl)ethenyl>-6-chloro-2-cyclohexenone

Guidance literature:: Multi-step reaction with 2 steps

1: 78.7 percent / DCC, H₃PO₄ / dimethylsulfoxide / 60 °C

2: 95.5 percent / CuCl₂*2H₂O, LiCl / dimethylformamide / 3 h / 80 °C

With phosphoric acid; dicyclohexyl-carbodiimide; lithium chloride; In dimethyl sulfoxide; N,N-dimethyl-formamide;