2-BENZYLSULFANYL-6-METHYL-[1,2,4]TRIAZOLO[1,5-A]PYRIMIDINE-5,7-DIOL

Base Information

Chemical Name:2-BENZYLSULFANYL-6-METHYL-[1,2,4]TRIAZOLO[1,5-A]PYRIMIDINE-5,7-DIOL
CAS No.:98968-32-2
Molecular Formula:C13H12 N4 O2 S
Molecular Weight:0
Hs Code.:
Mol file:98968-32-2.mol

Synonyms:2-BENZYLSULFANYL-6-METHYL-[1,2,4]TRIAZOLO[1,5-A]PYRIMIDINE-5,7-DIOL

Suppliers and Price of 2-BENZYLSULFANYL-6-METHYL-[1,2,4]TRIAZOLO[1,5-A]PYRIMIDINE-5,7-DIOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-BENZYLSULFANYL-6-METHYL-[1,2,4]-TRIAZOLO-[1,5-A]-PYRIMIDINE-5,7-DIOL 95.00%
5MG
$ 497.08

Total 3 raw suppliers

Chemical Property of 2-BENZYLSULFANYL-6-METHYL-[1,2,4]TRIAZOLO[1,5-A]PYRIMIDINE-5,7-DIOL

Chemical Property:

PSA：108.58000
LogP:1.72390

Purity/Quality:: 2-BENZYLSULFANYL-6-METHYL-[1,2,4]-TRIAZOLO-[1,5-A]-PYRIMIDINE-5,7-DIOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-BENZYLSULFANYL-6-METHYL-[1,2,4]TRIAZOLO[1,5-A]PYRIMIDINE-5,7-DIOL

There total 1 articles about 2-BENZYLSULFANYL-6-METHYL-[1,2,4]TRIAZOLO[1,5-A]PYRIMIDINE-5,7-DIOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 609-02-9
methyl-malonic acid dimethylester

: 3922-47-2
3-(benzylthio)-1H-1,2,4-triazol-5-amine

: 98968-32-2
2-benzylthio-5,7-dihydroxy-6-methyl-1,2,4-triazolo<1,5-a>pyrimidine

Guidance literature:: With sodium methylate; In methanol; for 96h; Heating;
DOI:10.1002/jhet.5570360127

Reference yield: 85.0%

: 98968-32-2
2-benzylthio-5,7-dihydroxy-6-methyl-1,2,4-triazolo<1,5-a>pyrimidine

: 98968-33-3
2-benzylthio-5,7-dichloro-6-methyl-1,2,4-triazolo<1,5-a>pyrimidine

Guidance literature:: With trichlorophosphate; In acetonitrile; for 28h; Heating;
DOI:10.1002/jhet.5570360127

Reference yield:

: 98968-32-2
2-benzylthio-5,7-dihydroxy-6-methyl-1,2,4-triazolo<1,5-a>pyrimidine

: 98968-35-5
2-benzylthio-5-methoxy-6-methyl-1,2,4-triazolo<1,5-a>pyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / POCl₃ / acetonitrile / 28 h / Heating

2: 74 percent / Zn-Cu, AcOH / methanol; tetrahydrofuran / 20 h / Ambient temperature

3: 65 percent / NaOMe / methanol / 0.33 h

With sodium methylate; copper; acetic acid; zinc; trichlorophosphate; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1002/jhet.5570360127