Isoxazole, 5-[2-(3-methoxyphenyl)-3-nitropropyl]-3-methyl-4-nitro-

Base Information

Chemical Name:Isoxazole, 5-[2-(3-methoxyphenyl)-3-nitropropyl]-3-methyl-4-nitro-
CAS No.:929719-06-2
Molecular Formula:C₁₄H₁₅N₃O₆
Molecular Weight:321.29
Hs Code.:
Mol file:929719-06-2.mol

Synonyms:Isoxazole, 5-[2-(3-methoxyphenyl)-3-nitropropyl]-3-methyl-4-nitro-

Suppliers and Price of Isoxazole, 5-[2-(3-methoxyphenyl)-3-nitropropyl]-3-methyl-4-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Isoxazole, 5-[2-(3-methoxyphenyl)-3-nitropropyl]-3-methyl-4-nitro-

Chemical Property:

Melting Point:112 - 114 °C (ethanol)
PSA：126.90000
LogP:3.54920

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Isoxazole, 5-[2-(3-methoxyphenyl)-3-nitropropyl]-3-methyl-4-nitro-

There total 3 articles about Isoxazole, 5-[2-(3-methoxyphenyl)-3-nitropropyl]-3-methyl-4-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-[(E)-2-(3-Methoxy-phenyl)-vinyl]-3-methyl-4-nitro-isoxazole

: 75-52-5
nitromethane

: 929719-06-2
5-[2-(3-methoxyphenyl)-3-nitropropyl]-3-methyl-4-nitroisoxazole

Guidance literature:: With piperidine; In ethanol; at 65 ℃; for 4h;
DOI:10.1016/j.tet.2006.12.044

Reference yield:

: 1123-49-5
3,5-dimethyl-4-nitroisoxazole

: 929719-06-2
5-[2-(3-methoxyphenyl)-3-nitropropyl]-3-methyl-4-nitroisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 2 h / 65 °C

2: piperidine / ethanol / 4 h / 65 °C

With piperidine; In ethanol; 1: Knoevenagel reaction / 2: Michael reaction;
DOI:10.1016/j.tet.2006.12.044

Reference yield:

: 591-31-1
3-methoxy-benzaldehyde

: 929719-06-2
5-[2-(3-methoxyphenyl)-3-nitropropyl]-3-methyl-4-nitroisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 2 h / 65 °C

2: piperidine / ethanol / 4 h / 65 °C

With piperidine; In ethanol; 1: Knoevenagel reaction / 2: Michael reaction;
DOI:10.1016/j.tet.2006.12.044