cyclo-[Orn(Nα-6-heptyloxy-2-naphthoyl)-Thr-Pro-hTyr-Lys(Nε-Cbz)-Pro(4S-N3)]

Base Information

Chemical Name:cyclo-[Orn(Nα-6-heptyloxy-2-naphthoyl)-Thr-Pro-hTyr-Lys(Nε-Cbz)-Pro(4S-N3)]
CAS No.:1203556-99-3
Molecular Formula:C₆₁H₇₉N₁₁O₁₂
Molecular Weight:1158.36
Hs Code.:

Synonyms:cyclo-[Orn(Nα-6-heptyloxy-2-naphthoyl)-Thr-Pro-hTyr-Lys(Nε-Cbz)-Pro(4S-N3)]

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Chemical Property of cyclo-[Orn(Nα-6-heptyloxy-2-naphthoyl)-Thr-Pro-hTyr-Lys(Nε-Cbz)-Pro(4S-N3)]

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Technology Process of cyclo-[Orn(Nα-6-heptyloxy-2-naphthoyl)-Thr-Pro-hTyr-Lys(Nε-Cbz)-Pro(4S-N3)]

There total 20 articles about cyclo-[Orn(Nα-6-heptyloxy-2-naphthoyl)-Thr-Pro-hTyr-Lys(Nε-Cbz)-Pro(4S-N3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₁H₈₁N₁₁O₁₃

: 1203556-99-3
cyclo-[Orn(Nα-6-heptyloxy-2-naphthoyl)-Thr-Pro-hTyr-Lys(Nε-Cbz)-Pro(4S-N3)]

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1016/j.ejmech.2012.01.054

Reference yield:

: C₃₃H₄₈N₄O₇

: 1203557-75-8
C₃₄H₄₅N₇O₉

: 1203556-99-3
cyclo-[Orn(Nα-6-heptyloxy-2-naphthoyl)-Thr-Pro-hTyr-Lys(Nε-Cbz)-Pro(4S-N3)]

Guidance literature:: C₃₃H₄₈N₄O₇; C₃₄H₄₅N₇O₉; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 10h;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h; Further stages;
DOI:10.1016/j.tet.2012.02.015

Reference yield:

: C₂₀H₃₆N₄O₇

: 1203556-99-3
cyclo-[Orn(Nα-6-heptyloxy-2-naphthoyl)-Thr-Pro-hTyr-Lys(Nε-Cbz)-Pro(4S-N3)]

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide / 24 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 20 °C

3.2: 1 h / 20 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.02.015