(±)-2-benzyl-9-methyl-2-azahexacyclo[10.6.6.0^1,5.0^6,11.0^13,18.0^19,24]-tetracosa-6(11),7,9,13,15,17,19(24),20,22-nonaen-3-one

Base Information

• Chemical Name: (±)-2-benzyl-9-methyl-2-azahexacyclo[10.6.6.0^1,5.0^6,11.0^13,18.0^19,24]-tetracosa-6(11),7,9,13,15,17,19(24),20,22-nonaen-3-one
• CAS No.: 1608141-08-7
• Molecular Formula: C₃₁H₂₅NO
• Molecular Weight: 427.546

Synonyms:(±)-2-benzyl-9-methyl-2-azahexacyclo[10.6.6.0^1,5.0^6,11.0^13,18.0^19,24]-tetracosa-6(11),7,9,13,15,17,19(24),20,22-nonaen-3-one

Chemical Property of (±)-2-benzyl-9-methyl-2-azahexacyclo[10.6.6.0^1,5.0^6,11.0^13,18.0^19,24]-tetracosa-6(11),7,9,13,15,17,19(24),20,22-nonaen-3-one

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Technology Process of (±)-2-benzyl-9-methyl-2-azahexacyclo[10.6.6.0^1,5.0^6,11.0^13,18.0^19,24]-tetracosa-6(11),7,9,13,15,17,19(24),20,22-nonaen-3-one

There total 4 articles about (±)-2-benzyl-9-methyl-2-azahexacyclo[10.6.6.0^1,5.0^6,11.0^13,18.0^19,24]-tetracosa-6(11),7,9,13,15,17,19(24),20,22-nonaen-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

N-benzyl-N-(4-methylcinnamoyl)-9-aminoanthracene → (±)-2-benzyl-9-methyl-2-azahexacyclo[10.6.6.01,5.06,11.013,18.019,24]-tetracosa-6(11),7,9,13,15,17,19(24),20,22-nonaen-3-one (1608141-08-7)

Guidance literature:

With polyphosphoric acid; In chloroform; at 120 ℃; for 2h;

DOI:10.1039/c4ob00411f

Reference yield:

N-(4-methylcinnamoyl)-9-aminoanthracene → (±)-2-benzyl-9-methyl-2-azahexacyclo[10.6.6.01,5.06,11.013,18.019,24]-tetracosa-6(11),7,9,13,15,17,19(24),20,22-nonaen-3-one (1608141-08-7)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 2 h / Reflux

2: polyphosphoric acid / chloroform / 2 h / 120 °C

With potassium tert-butylate; In tetrahydrofuran; chloroform;

DOI:10.1039/c4ob00411f

Reference yield:

4-methylcinnamoyl chloride (13565-07-6,15851-89-5) → (±)-2-benzyl-9-methyl-2-azahexacyclo[10.6.6.01,5.06,11.013,18.019,24]-tetracosa-6(11),7,9,13,15,17,19(24),20,22-nonaen-3-one (1608141-08-7)

Guidance literature:

Multi-step reaction with 3 steps

1: N,N-diethylaniline / ethyl acetate / 1 h / 60 °C

2: potassium tert-butylate / tetrahydrofuran / 2 h / Reflux

3: polyphosphoric acid / chloroform / 2 h / 120 °C

With potassium tert-butylate; N,N-diethylaniline; In tetrahydrofuran; chloroform; ethyl acetate;

DOI:10.1039/c4ob00411f

upstream raw materials:

4-methylcinnamic acid

4-methylcinnamoyl chloride

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