3-Cyclohexene-1-carboxylicacid,6-amino-,(1S,6R)-(9CI)

Base Information

Chemical Name:3-Cyclohexene-1-carboxylicacid,6-amino-,(1S,6R)-(9CI)
CAS No.:98856-64-5
Molecular Formula:C7H11 N O2
Molecular Weight:141.17
Hs Code.:
Mol file:98856-64-5.mol

Synonyms:3-Cyclohexene-1-carboxylicacid, 6-amino-, (1S-cis)-; (1S,2R)-2-Amino-4-cyclohexene-1-carboxylic acid;cis-(1S,2R)-2-Amino-4-cyclohexene-1-carboxylic acid

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Cyclohexene-1-carboxylicacid,6-amino-,(1S,6R)-(9CI)

Chemical Property:

PSA：63.32000
LogP:1.06480

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Cyclohexene-1-carboxylicacid,6-amino-,(1S,6R)-(9CI)

There total 22 articles about 3-Cyclohexene-1-carboxylicacid,6-amino-,(1S,6R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 109577-02-8
methyl (1S,2R)-2-<(2-methylsulfonyl)ethoxycarbonylamino>-1-cyclohex-4-ene carboxylate

: 98856-64-5,189125-31-3
(1S,2R)-2-amino-1-cyclohex-4-ene carboxylic acid

Guidance literature:: With sodium hydroxide;
DOI:10.1016/S0040-4039(00)83870-8

Reference yield: 69.0%

: 85-40-5
1,2,3,6-tertahydrophthalimide

: 54162-90-2,74952-21-9,97945-19-2,98856-64-5,128441-32-7,189125-31-3
(cis)-6-aminocyclohex-3-ene-1-carboxylic acid

Guidance literature:: With trichloroisocyanuric acid; sodium hydroxide; In water; at 0 ℃; for 1.5h; Reflux;
DOI:10.1016/j.tetlet.2021.153422

Reference yield:

: 31139-02-3,31139-03-4,56124-48-2,88335-93-7,88335-94-8,93603-11-3
(1R,6S)-6-methoxycarbonyl-3-cyclohexene-1-carboxylic acid

: 98856-64-5,189125-31-3
(1S,2R)-2-amino-1-cyclohex-4-ene carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

2: 76 percent / 1 N sodium hydroxide / methanol; H₂O / 16 h

With sodium hydroxide; In methanol; water;
DOI:10.1248/cpb.35.996