N-Cyclohexyl-N-((E)-2-methyl-3-phenylsulfanyl-propenyl)-3-oxo-butyramide

Base Information

• Chemical Name: N-Cyclohexyl-N-((E)-2-methyl-3-phenylsulfanyl-propenyl)-3-oxo-butyramide
• CAS No.: 799280-53-8
• Molecular Formula: C₂₀H₂₇NO₂S
• Molecular Weight: 345.506

Synonyms:N-Cyclohexyl-N-((E)-2-methyl-3-phenylsulfanyl-propenyl)-3-oxo-butyramide

Chemical Property of N-Cyclohexyl-N-((E)-2-methyl-3-phenylsulfanyl-propenyl)-3-oxo-butyramide

Chemical Property:

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Technology Process of N-Cyclohexyl-N-((E)-2-methyl-3-phenylsulfanyl-propenyl)-3-oxo-butyramide

There total 3 articles about N-Cyclohexyl-N-((E)-2-methyl-3-phenylsulfanyl-propenyl)-3-oxo-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiophenol (108-98-5) → N-Cyclohexyl-N-((E)-2-methyl-3-phenylsulfanyl-propenyl)-3-oxo-butyramide (799280-53-8)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 1 h / 0 °C

2: Al₂O₃ / 2 h / Ambient temperature

3: Heating

With aluminum oxide; triethylamine; In dichloromethane;

DOI:10.1016/S0040-4020(98)83055-X

Reference yield:

2-methyl-3-(phenylsulfanyl)propanal (56102-14-8,173167-75-4) → N-Cyclohexyl-N-((E)-2-methyl-3-phenylsulfanyl-propenyl)-3-oxo-butyramide (799280-53-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Al₂O₃ / 2 h / Ambient temperature

2: Heating

With aluminum oxide;

DOI:10.1016/S0040-4020(98)83055-X

Reference yield:

2,2,6-trimethyl-4H-1,3-dioxin-4-one (5394-63-8) + Cyclohexyl-[2-methyl-3-phenylsulfanyl-prop-(E)-ylidene]-amine → N-Cyclohexyl-N-((E)-2-methyl-3-phenylsulfanyl-propenyl)-3-oxo-butyramide (799280-53-8)

Guidance literature:

Heating;

DOI:10.1016/S0040-4020(98)83055-X

upstream raw materials:

2,2,6-trimethyl-4H-1,3-dioxin-4-one

2-methyl-3-(phenylsulfanyl)propanal

thiophenol

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