(1S,2S,5R,6R)-3,8-Bis-(4-methoxy-phenyl)-4,7-dimethyl-tricyclo[4.2.2.0^2,5]deca-3,7-diene

Base Information

• Chemical Name: (1S,2S,5R,6R)-3,8-Bis-(4-methoxy-phenyl)-4,7-dimethyl-tricyclo[4.2.2.0^2,5]deca-3,7-diene
• CAS No.: 66606-89-1
• Molecular Formula: C₂₆H₂₈O₂
• Molecular Weight: 372.507

Synonyms:(1S,2S,5R,6R)-3,8-Bis-(4-methoxy-phenyl)-4,7-dimethyl-tricyclo[4.2.2.0^2,5]deca-3,7-diene

Chemical Property of (1S,2S,5R,6R)-3,8-Bis-(4-methoxy-phenyl)-4,7-dimethyl-tricyclo[4.2.2.0^2,5]deca-3,7-diene

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Technology Process of (1S,2S,5R,6R)-3,8-Bis-(4-methoxy-phenyl)-4,7-dimethyl-tricyclo[4.2.2.0^2,5]deca-3,7-diene

There total 6 articles about (1S,2S,5R,6R)-3,8-Bis-(4-methoxy-phenyl)-4,7-dimethyl-tricyclo[4.2.2.0^2,5]deca-3,7-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C26H28O2 (66606-92-6) → (1S,2S,5R,6R)-3,8-Bis-(4-methoxy-phenyl)-4,7-dimethyl-tricyclo[4.2.2.02,5]deca-3,7-diene (66606-89-1)

Guidance literature:

With p-benzoquinone; In acetonitrile; at 23 ℃; for 0.25h; Product distribution; Mechanism; Quantum yield; Irradiation; reaction quenchers (piperilene, Et₃N); other weak electron acceptor (9,10-anthraquinone); other reaction types under other conditions (without irradiation, in presence of various quinones or tetracyanoethylene); a series of phenylated cage compounds;

DOI:10.1021/ja00393a029

Reference yield: 88.0%

C26H28O2 (66606-92-6) → (1S,2S,5R,6R)-3,8-Bis-(4-methoxy-phenyl)-4,7-dimethyl-tricyclo[4.2.2.02,5]deca-3,7-diene (66606-89-1)

Guidance literature:

With tetraethylammonium perchlorate; In acetonitrile; for 0.166667h; anodic oxidation with Pt gauze electrode;

DOI:10.1246/cl.1984.1553

Reference yield:

C26H28O2 (66606-92-6) → (1S,2S,5R,6R)-3,8-Bis-(4-methoxy-phenyl)-4,7-dimethyl-tricyclo[4.2.2.02,5]deca-3,7-diene (66606-89-1)

Guidance literature:

With phenanthrene-9,10-dicarbonitrile; In benzene; Irradiation;

DOI:10.1021/ja00334a070

upstream raw materials:

C₂₆H₂₈O₂

C₃₂H₂₈N₄O₂

C₂₆H₂₈O₂

C₂₆H₂₈O₂

Downstream raw materials:

C₃₂H₂₈N₄O₂

C₂₆H₂₈O₂

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