Technology Process of C28H46O5Si
There total 6 articles about C28H46O5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate; Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
DOI:10.1016/j.tet.2011.02.061
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap; triethylamine / dichloromethane / -10 °C / Inert atmosphere
2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C
With
dmap; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine;
In
dichloromethane;
DOI:10.1016/j.tet.2011.02.061
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydroxide / tetrahydrofuran; water / 40 °C
1.2: 20 °C
2.1: triethyl borane; oxygen; tri-n-butyl-tin hydride / toluene / -30 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
4.1: dmap; triethylamine / dichloromethane / -10 °C / Inert atmosphere
5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C
With
dmap; lithium aluminium tetrahydride; triethyl borane; oxygen; tri-n-butyl-tin hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1016/j.tet.2011.02.061