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C28H46O5Si

Base Information
  • Chemical Name:C28H46O5Si
  • CAS No.:1300040-18-9
  • Molecular Formula:C28H46O5Si
  • Molecular Weight:490.756
  • Hs Code.:
C<sub>28</sub>H<sub>46</sub>O<sub>5</sub>Si

Synonyms:C28H46O5Si

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Chemical Property of C28H46O5Si
Chemical Property:
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Technology Process of C28H46O5Si

There total 6 articles about C28H46O5Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2011.02.061
Guidance literature:
Multi-step reaction with 2 steps
1: dmap; triethylamine / dichloromethane / -10 °C / Inert atmosphere
2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C
With dmap; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; In dichloromethane;
DOI:10.1016/j.tet.2011.02.061
Guidance literature:
Multi-step reaction with 5 steps
1.1: sodium hydroxide / tetrahydrofuran; water / 40 °C
1.2: 20 °C
2.1: triethyl borane; oxygen; tri-n-butyl-tin hydride / toluene / -30 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
4.1: dmap; triethylamine / dichloromethane / -10 °C / Inert atmosphere
5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C
With dmap; lithium aluminium tetrahydride; triethyl borane; oxygen; tri-n-butyl-tin hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1016/j.tet.2011.02.061
upstream raw materials:

C23H32O5

C28H48O5Si

C22H30O5

t-butyldimethylsiyl triflate

Downstream raw materials:

C30H52O6Si

C24H38O6

C24H36O6

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