N-(2,2-diethoxyethyl)-4-methyl-N-(3-phenyl-prop-2-ynyl)benzenesulfonamide

Base Information

• Chemical Name: N-(2,2-diethoxyethyl)-4-methyl-N-(3-phenyl-prop-2-ynyl)benzenesulfonamide
• CAS No.: 1149618-37-0
• Molecular Formula: C₂₂H₂₇NO₄S
• Molecular Weight: 401.527

Synonyms:N-(2,2-diethoxyethyl)-4-methyl-N-(3-phenyl-prop-2-ynyl)benzenesulfonamide

Chemical Property of N-(2,2-diethoxyethyl)-4-methyl-N-(3-phenyl-prop-2-ynyl)benzenesulfonamide

Chemical Property:

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Technology Process of N-(2,2-diethoxyethyl)-4-methyl-N-(3-phenyl-prop-2-ynyl)benzenesulfonamide

There total 1 articles about N-(2,2-diethoxyethyl)-4-methyl-N-(3-phenyl-prop-2-ynyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

N-(2,2-diethoxy-ethyl)-4-methylbenzenesulfonamide (40597-44-2) + 1-bromo-3-phenylprop-2-yne (1794-48-5) → N-(2,2-diethoxyethyl)-4-methyl-N-(3-phenyl-prop-2-ynyl)benzenesulfonamide (1149618-37-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol9005689

Reference yield: 90.0%

N-(2,2-diethoxyethyl)-4-methyl-N-(3-phenyl-prop-2-ynyl)benzenesulfonamide (1149618-37-0) → 3-(bromo(phenyl)methylene)-4-ethoxy-1-(toluene-4-sulfonyl)pyrrolidine (1149618-63-2)

Guidance literature:

With ferric(III) bromide; In dichloromethane; at 0 ℃; for 0.5h; stereoselective reaction; Inert atmosphere;

DOI:10.1021/ol9005689

Reference yield: 87.0%

N-(2,2-diethoxyethyl)-4-methyl-N-(3-phenyl-prop-2-ynyl)benzenesulfonamide (1149618-37-0) → phenyl[1-(toluene-4-sulfonyl)-2,5-dihydro-1H-pyrrol-3-yl]methanone

Guidance literature:

With iron(III) chloride hexahydrate; In acetone; at 50 ℃; for 1.5h;

DOI:10.1002/chem.201000686

upstream raw materials:

N-(2,2-diethoxy-ethyl)-4-methylbenzenesulfonamide

1-bromo-3-phenylprop-2-yne

Downstream raw materials:

3-(bromo(phenyl)methylene)-4-ethoxy-1-(toluene-4-sulfonyl)pyrrolidine

3-bromo-4-(bromo-(phenyl)-methylene)-1-(toluene-4-sulfonyl)pyrrolidine

C₂₀H₂₂ClNO₃S

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