C₃₀H₃₉NO₈

Base Information

Chemical Name:C₃₀H₃₉NO₈
CAS No.:1359021-70-7
Molecular Formula:C₃₀H₃₉NO₈
Molecular Weight:541.642
Hs Code.:

C<sub>30</sub>H<sub>39</sub>NO<sub>8</sub>

Synonyms:C₃₀H₃₉NO₈

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Chemical Property of C₃₀H₃₉NO₈

Chemical Property:

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Technology Process of C₃₀H₃₉NO₈

There total 16 articles about C₃₀H₃₉NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1359021-69-4
C₂₅H₃₁NO₆

: 1359021-70-7
C₃₀H₃₉NO₈

Guidance literature:: dmap; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 50868-73-0
2-methoxy-6-methylbenzeneamine

: 1359021-70-7
C₃₀H₃₉NO₈

Guidance literature:: Multi-step reaction with 14 steps

1.1: bromine; acetic acid / methanol / 2 h / 20 °C / Cooling with ice

2.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

2.2: 4 h / 0 - 50 °C

3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

3.2: 1 h / 20 °C

4.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

4.2: pH 1

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

6.1: triethylamine / dmap / 1 h / 20 °C

7.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

7.2: 0.33 h / 20 °C

8.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 17 h / 0 - 20 °C

8.2: 0.33 h / 20 °C

9.1: dmap / dichloromethane / 0.33 h / 20 °C

10.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 0.5 h / 0 °C

10.2: 1 h / -78 - -5 °C / Inert atmosphere

11.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

12.1: dmap / dichloromethane / 0.5 h / 20 °C

13.1: methanol; sodium tetrahydroborate / 0.5 h / 0 - 20 °C

14.1: dmap / dichloromethane / 0.5 h / 20 °C

With hydrogenchloride; methanol; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; [bis(acetoxy)iodo]benzene; bromine; isopropylmagnesium chloride; boron tribromide; diisobutylaluminium hydride; acetic acid; triethylamine; trifluoroacetic acid; lithium chloride; sodium nitrite; dmap; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; toluene; tert-butyl alcohol;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1359021-70-7
C₃₀H₃₉NO₈

Guidance literature:: Multi-step reaction with 12 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

1.2: 1 h / 20 °C

2.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: triethylamine / dmap / 1 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

5.2: 0.33 h / 20 °C

6.1: [bis(acetoxy)iodo]benzene / 1,4-dioxane / 17 h / 0 - 20 °C

6.2: 0.33 h / 20 °C

7.1: dmap / dichloromethane / 0.33 h / 20 °C

8.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 0.5 h / 0 °C

8.2: 1 h / -78 - -5 °C / Inert atmosphere

9.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

10.1: dmap / dichloromethane / 0.5 h / 20 °C

11.1: methanol; sodium tetrahydroborate / 0.5 h / 0 - 20 °C

12.1: dmap / dichloromethane / 0.5 h / 20 °C

With methanol; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; [bis(acetoxy)iodo]benzene; isopropylmagnesium chloride; boron tribromide; diisobutylaluminium hydride; triethylamine; trifluoroacetic acid; lithium chloride; dmap; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; tert-butyl alcohol;