1-formyl-4-phenyl-1,2,3,6-tetrahydropyridine-1-13C

Base Information

Chemical Name:1-formyl-4-phenyl-1,2,3,6-tetrahydropyridine-1-13C
CAS No.:929533-03-9
Molecular Formula:C₁₂H₁₃NO
Molecular Weight:188.23
Hs Code.:

Synonyms:1-formyl-4-phenyl-1,2,3,6-tetrahydropyridine-1-13C

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Chemical Property of 1-formyl-4-phenyl-1,2,3,6-tetrahydropyridine-1-13C

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Technology Process of 1-formyl-4-phenyl-1,2,3,6-tetrahydropyridine-1-13C

There total 1 articles about 1-formyl-4-phenyl-1,2,3,6-tetrahydropyridine-1-13C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 10338-69-9
1,2,3,6-tetrahydro-4-phenylpyridine

: 73222-61-4
<1-¹³C>-Ameisensaeure-ethylester

: 929533-03-9
1-formyl-4-phenyl-1,2,3,6-tetrahydropyridine-1-13C

Guidance literature:: In acetonitrile; at 60 ℃; for 36h;
DOI:10.1002/jms.1135

Reference yield:

: 929533-03-9
1-formyl-4-phenyl-1,2,3,6-tetrahydropyridine-1-13C

: 3675-63-6
bromoethane-d5

: 929533-04-0
1-cyclopropyl-1-13C-2,2,3,3-d4-4-phenyl-1,2,3,6-tetrahydropyridine

Guidance literature:: bromoethane-d5; With magnesium; In tetrahydrofuran; for 3h; Heating;

1-formyl-4-phenyl-1,2,3,6-tetrahydropyridine-1-13C; With titanium(IV) isopropylate; In tetrahydrofuran; at 60 ℃; for 18h;
DOI:10.1002/jms.1135

Reference yield:

: 929533-03-9
1-formyl-4-phenyl-1,2,3,6-tetrahydropyridine-1-13C

: 929533-06-2
C₁₃⁽¹³⁾CH₁₃⁽²⁾H₄NO

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran / 3 h / Heating

1.2: Ti(iOPr)4 / tetrahydrofuran / 18 h / 60 °C

2.1: m-chloroperoxobenzoic acid / CH₂Cl₂ / 0.33 h / 0 °C

With magnesium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/jms.1135