{(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}⁽²⁺⁾*2B(C₆H₅)4^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}(B(C₆H₅)4)2

Base Information

• Chemical Name: {(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}⁽²⁺⁾*2B(C₆H₅)4^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}(B(C₆H₅)4)2
• CAS No.: 110391-76-9
• Molecular Formula: 2C₂₄H₂₀B*C₄₈H₅₅P₄RhSe₂
• Molecular Weight: 1655.15

Synonyms:{(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}⁽²⁺⁾*2B(C₆H₅)4^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}(B(C₆H₅)4)2

Chemical Property of {(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}⁽²⁺⁾*2B(C₆H₅)4^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}(B(C₆H₅)4)2

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Technology Process of {(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}⁽²⁺⁾*2B(C₆H₅)4^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}(B(C₆H₅)4)2

There total 1 articles about {(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}⁽²⁺⁾*2B(C₆H₅)4^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)Rh(Se₂CHP(C₂H₅)3)}(B(C₆H₅)4)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(triphos)RhCl(Se2CPEt3) + sodium tetraphenyl borate (143-66-8) → {(CH3C(CH2P(C6H5)2)3)Rh(Se2CHP(C2H5)3)}(2+)*2B(C6H5)4(1-)={(CH3C(CH2P(C6H5)2)3)Rh(Se2CHP(C2H5)3)}(B(C6H5)4)2 (110391-76-9)

Guidance literature:

With HSO₃CF₃ or HBF₄*O(C₂H₅)2; In tetrahydrofuran; an equivalent amt. of HSO3CF3 or HBF4*OEt2 was added to a soln. of ((triphos)RhCl(Se2CPEt3)) in THF containing NaBPh4; mechanism discussed;; ppt. after standing for 1 h; dried in a stream of N2;;

Reference yield:

{(CH3C(CH2P(C6H5)2)3)Rh(Se2CHP(C2H5)3)}(2+)*2B(C6H5)4(1-)={(CH3C(CH2P(C6H5)2)3)Rh(Se2CHP(C2H5)3)}(B(C6H5)4)2 (110391-76-9) → {(triphos)Rh(Se2CO)}{BPh4} (97689-99-1)

Guidance literature:

With O₂; In dichloromethane; N,N-dimethyl-formamide; oxygen was bubbled through a soln. of ((triphos)Rh(Se2CHPEt3))(BPh4)2 in DMF-CH2Cl2 for 15 min.; mechanism discussed;; pptn. by addn. of a 3:1 mixt. of ethanol and n-hexane and partial evapn. of the solvents; dried in a stream of N2;;

upstream raw materials:

sodium tetraphenyl borate

Downstream raw materials:

{(triphos)Rh(Se₂CO)}{BPh₄}

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