Boc-Tyr-Gly-Aib-1-aminoindan

Base Information

Chemical Name:Boc-Tyr-Gly-Aib-1-aminoindan
CAS No.:74814-23-6
Molecular Formula:C₂₉H₃₈N₄O₆
Molecular Weight:538.644
Hs Code.:

Synonyms:Boc-Tyr-Gly-Aib-1-aminoindan

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Chemical Property of Boc-Tyr-Gly-Aib-1-aminoindan

Chemical Property:

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Technology Process of Boc-Tyr-Gly-Aib-1-aminoindan

There total 4 articles about Boc-Tyr-Gly-Aib-1-aminoindan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 3978-80-1
Boc-Tyr-OH

: 74814-22-5
Gly-Aib-1-aminoindan hydrochloride

: 74814-23-6
Boc-Tyr-Gly-Aib-1-aminoindan

Guidance literature:: With diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; at 0 - 25 ℃; for 52h;
DOI:10.1021/jm00184a010

Reference yield:

: 134269-28-6
Boc-Gly-Aib-OBzl

: 74814-23-6
Boc-Tyr-Gly-Aib-1-aminoindan

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / H₂ / 10percent Pd/C / methanol / 2068.6 Torr

2: 51 percent / Et₃N, diphenylphosphoryl azide (DPPA) / dimethylformamide / 52 h / 0 - 25 °C

3: 4 N aq. HCl / dioxane / 3 h / 25 °C

4: 65 percent / Et₃N, diphenylphosphoryl azide (DPPA) / dimethylformamide / 52 h / 0 - 25 °C

With hydrogenchloride; diphenylphosphoranyl azide; hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00184a010

Reference yield:

: 74814-21-4
tert-butlyoxycarbonyl-Gly-Aib-OH

: 74814-23-6
Boc-Tyr-Gly-Aib-1-aminoindan

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / Et₃N, diphenylphosphoryl azide (DPPA) / dimethylformamide / 52 h / 0 - 25 °C

2: 4 N aq. HCl / dioxane / 3 h / 25 °C

3: 65 percent / Et₃N, diphenylphosphoryl azide (DPPA) / dimethylformamide / 52 h / 0 - 25 °C

With hydrogenchloride; diphenylphosphoranyl azide; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jm00184a010