methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-α-D-glucopyranoside
CAS No.:1338712-09-6
Molecular Formula:C₆₃H₆₂O₁₅
Molecular Weight:1059.18
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-α-D-glucopyranoside

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Chemical Property of methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-α-D-glucopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-α-D-glucopyranoside

There total 4 articles about methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1338712-06-3
methyl 2,3,4-tri-O-benzyl-6-O-pentenoyl-α-D-glucopyranoside

: 1338712-01-8
ethyl 2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-1-thio-β-D-glucopyranoside

: 1338712-09-6
methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: methyl 2,3,4-tri-O-benzyl-6-O-pentenoyl-α-D-glucopyranoside; With N-iodo-succinimide; trifluorormethanesulfonic acid; water; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 0.166667h;

In 1,2-dichloro-ethane; at 20 ℃; for 0.333333h; Molecular sieve;

ethyl 2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-1-thio-β-D-glucopyranoside; In 1,2-dichloro-ethane; at 20 ℃; for 2h; Molecular sieve;
DOI:10.1039/c1cc13409d

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 1338712-09-6
methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: dicyclohexyl-carbodiimide / dichloromethane / 19 h / 0 - 20 °C

2.1: N-iodo-succinimide; trifluorormethanesulfonic acid; water / 1,2-dichloro-ethane / 0.17 h / 0 - 20 °C

2.2: 0.33 h / 20 °C / Molecular sieve

2.3: 2 h / 20 °C / Molecular sieve

With N-iodo-succinimide; trifluorormethanesulfonic acid; water; dicyclohexyl-carbodiimide; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1039/c1cc13409d

Reference yield:

: 35784-51-1
ethyl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside

: 1338712-09-6
methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 3 h / 0 °C

2.1: N-iodo-succinimide; trifluorormethanesulfonic acid; water / 1,2-dichloro-ethane / 0.17 h / 0 - 20 °C

2.2: 0.33 h / 20 °C / Molecular sieve

2.3: 2 h / 20 °C / Molecular sieve

With N-iodo-succinimide; trifluorormethanesulfonic acid; water; sodium hydride; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1039/c1cc13409d