triphenylbismuthonio-4,4-dimethyl-2,6-dioxocyclohexane-1-ide

Base Information

Chemical Name:triphenylbismuthonio-4,4-dimethyl-2,6-dioxocyclohexane-1-ide
CAS No.:105071-90-7
Molecular Formula:C₂₆H₂₅BiO₂
Molecular Weight:578.464
Hs Code.:

Synonyms:triphenylbismuthonio-4,4-dimethyl-2,6-dioxocyclohexane-1-ide

Suppliers and Price of triphenylbismuthonio-4,4-dimethyl-2,6-dioxocyclohexane-1-ide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of triphenylbismuthonio-4,4-dimethyl-2,6-dioxocyclohexane-1-ide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of triphenylbismuthonio-4,4-dimethyl-2,6-dioxocyclohexane-1-ide

There total 5 articles about triphenylbismuthonio-4,4-dimethyl-2,6-dioxocyclohexane-1-ide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 7173-99-1
triphenylbismuthine oxide

: 126-81-8
dimedone

: 105071-90-7
triphenylbismuthonio-4,4-dimethyl-2,6-dioxocyclohexane-1-ide

Guidance literature:: With sodium hydride; In tetrahydrofuran; (N2); to suspn. of dione and NaH was added OBiPh3 at room temp., mixt. was kept until clear soln. was obtained; chromy. (silica-gel; 1% MeOH/CH2Cl2);
DOI:10.1039/c39890001749

Reference yield: 83.0%

: triphenylbismuth carbonate

: 126-81-8
dimedone

: 105071-90-7
triphenylbismuthonio-4,4-dimethyl-2,6-dioxocyclohexane-1-ide

Guidance literature:: In neat (no solvent); fractional crystn. from benzene-hexane;
DOI:10.1246/cl.1988.847

Reference yield: 75.0%

: 126-81-8
dimedone

: 47252-14-2
triphenylbismuth carbonate

: 105071-90-7
triphenylbismuthonio-4,4-dimethyl-2,6-dioxocyclohexane-1-ide

Guidance literature:: In dichloromethane; under Ar, stirred at 40°C for 3 h; filtered through celite, evapd., column chromy. with ether/hexane, elem. anal.;