9-(3'-azido-5'-O-tert-butyldiphenylsilyl-3'-deoxy-β-D-xylofuranos-1-yl)-6-N-(di-n-butylamino)methyleneadenine

Base Information

Chemical Name:9-(3'-azido-5'-O-tert-butyldiphenylsilyl-3'-deoxy-β-D-xylofuranos-1-yl)-6-N-(di-n-butylamino)methyleneadenine
CAS No.:1092106-44-9
Molecular Formula:C₃₅H₄₇N₉O₃Si
Molecular Weight:669.902
Hs Code.:

Synonyms:9-(3'-azido-5'-O-tert-butyldiphenylsilyl-3'-deoxy-β-D-xylofuranos-1-yl)-6-N-(di-n-butylamino)methyleneadenine

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Chemical Property of 9-(3'-azido-5'-O-tert-butyldiphenylsilyl-3'-deoxy-β-D-xylofuranos-1-yl)-6-N-(di-n-butylamino)methyleneadenine

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Technology Process of 9-(3'-azido-5'-O-tert-butyldiphenylsilyl-3'-deoxy-β-D-xylofuranos-1-yl)-6-N-(di-n-butylamino)methyleneadenine

There total 1 articles about 9-(3'-azido-5'-O-tert-butyldiphenylsilyl-3'-deoxy-β-D-xylofuranos-1-yl)-6-N-(di-n-butylamino)methyleneadenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 68950-21-0
9-(3'-azido-5'-O-tert-butyldiphenylsilyl-3'-deoxy-β-D-xylofuranos-1-yl)adenine

: 19449-30-0
N,N-dibutylformamide dimethyl acetal

: 1092106-44-9
9-(3'-azido-5'-O-tert-butyldiphenylsilyl-3'-deoxy-β-D-xylofuranos-1-yl)-6-N-(di-n-butylamino)methyleneadenine

Guidance literature:: In methanol; Heating;
DOI:10.1055/s-2008-1078025

Reference yield: 83.0%

: 1092106-44-9
9-(3'-azido-5'-O-tert-butyldiphenylsilyl-3'-deoxy-β-D-xylofuranos-1-yl)-6-N-(di-n-butylamino)methyleneadenine

: 77128-72-4,201335-88-8
N-(9-fluorenylmethoxycarbonyl)-O-methyl-L-tyrosine

: 9-[5'-O-tert-butyldiphenylsilyl-3'-N-(α-N-fluorenylmethoxycarbonyl-p-methoxy-L-phenylalanyl)amido-3'-deoxy-β-D-xylofuranos-1-yl]-6-N-(di-n-butylamino)methyleneadenine

Guidance literature:: N-(9-fluorenylmethoxycarbonyl)-O-methyl-L-tyrosine; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; at 0 ℃; Inert atmosphere;

9-(3'-azido-5'-O-tert-butyldiphenylsilyl-3'-deoxy-β-D-xylofuranos-1-yl)-6-N-(di-n-butylamino)methyleneadenine; With trimethylphosphane; In tetrahydrofuran; at 20 ℃;
DOI:10.1055/s-2008-1078025