benzyloxyacetic acid 3-[allyl-(toluene-4-sulfonyl)-amino]-1-methyl-allyl ester

Base Information

Chemical Name:benzyloxyacetic acid 3-[allyl-(toluene-4-sulfonyl)-amino]-1-methyl-allyl ester
CAS No.:1357059-24-5
Molecular Formula:C₂₃H₂₇NO₅S
Molecular Weight:429.537
Hs Code.:

Synonyms:benzyloxyacetic acid 3-[allyl-(toluene-4-sulfonyl)-amino]-1-methyl-allyl ester

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Chemical Property of benzyloxyacetic acid 3-[allyl-(toluene-4-sulfonyl)-amino]-1-methyl-allyl ester

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Technology Process of benzyloxyacetic acid 3-[allyl-(toluene-4-sulfonyl)-amino]-1-methyl-allyl ester

There total 2 articles about benzyloxyacetic acid 3-[allyl-(toluene-4-sulfonyl)-amino]-1-methyl-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 30379-55-6
benzyloxyacetic acid

: 1357059-20-1
(E)-N-allyl-N-(3-hydroxybut-1-enyl)-4-methylbenzenesulfonamide

: 1357059-24-5
benzyloxyacetic acid 3-[allyl-(toluene-4-sulfonyl)-amino]-1-methyl-allyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 15h; Inert atmosphere;
DOI:10.1039/c2ob06853b

Reference yield:

: 1357059-18-7
(E)-N-allyl-4-N-(3-oxobut-1-enyl)-4-methylbenzenesulfonamide

: 1357059-24-5
benzyloxyacetic acid 3-[allyl-(toluene-4-sulfonyl)-amino]-1-methyl-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / tetrahydrofuran; methanol / 12 h / 0 - 20 °C / Inert atmosphere

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 15 h / 0 - 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c2ob06853b