C₄₇H₇₅N₅O₁₂

Base Information

Chemical Name:C₄₇H₇₅N₅O₁₂
CAS No.:1610850-47-9
Molecular Formula:C₄₇H₇₅N₅O₁₂
Molecular Weight:902.139
Hs Code.:

C<sub>47</sub>H<sub>75</sub>N<sub>5</sub>O<sub>12</sub>

Synonyms:C₄₇H₇₅N₅O₁₂

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Chemical Property of C₄₇H₇₅N₅O₁₂

Chemical Property:

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Technology Process of C₄₇H₇₅N₅O₁₂

There total 25 articles about C₄₇H₇₅N₅O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610850-91-3
C₅₄H₈₁N₅O₁₂

: 1610850-47-9
C₄₇H₇₅N₅O₁₂

Guidance literature:: With triethylsilane; triethylamine; palladium dichloride; In dichloromethane; at 0 ℃; for 0.25h;
DOI:10.1016/j.tetlet.2014.04.079

Reference yield:

: 1610850-49-1
(S)-methyl 2-((2S,3S)-2-(tert-butoxycarbonylamino)-N,3-dimethylpentanamido)propanoate

: 1610850-47-9
C₄₇H₇₅N₅O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: dichloromethane / 2 h / 0 - 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C

2.2: 8 h / 20 °C

3.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 1 h / 0 - 20 °C

4.1: triethylamine; dmap / dichloromethane / 4 h / 0 - 20 °C

5.1: dichloromethane / 2 h

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C

6.2: 8 h / 20 °C

7.1: pyridine hydrogenfluoride / tetrahydrofuran / 2 h / 0 °C

8.1: triethylamine; palladium dichloride; triethylsilane / dichloromethane / 0.25 h / 0 °C

With triethylsilane; dmap; lithium hydroxide monohydrate; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium dichloride; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.tetlet.2014.04.079

Reference yield:

: 1610850-62-8
(2S,3R,E)-3-(tert-butyldimethylsilyloxy)-2,4-dimethylhex-4-en-1-ol

: 1610850-47-9
C₄₇H₇₅N₅O₁₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

2.1: di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 0.17 h / 0 °C

2.2: 0.75 h / -78 - 0 °C

2.3: 2 h / -78 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C

4.1: lithium borohydride / tetrahydrofuran; methanol / 1 h / 0 °C

5.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

6.1: N-ethyl-N,N-diisopropylamine; lithium chloride / acetonitrile / 0.33 h / 20 °C

6.2: 20 h / 20 °C

7.1: triethylamine; palladium dichloride; triethylsilane / dichloromethane / 0.25 h / 0 °C

8.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C

8.2: 8 h / 20 °C

9.1: pyridine hydrogenfluoride / tetrahydrofuran / 2 h / 0 °C

10.1: triethylamine; palladium dichloride; triethylsilane / dichloromethane / 0.25 h / 0 °C

With triethylsilane; lithium borohydride; di-n-butylboryl trifluoromethanesulfonate; sulfur trioxide pyridine complex; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; palladium dichloride; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.tetlet.2014.04.079