[bis(N-(2,6-diisopropylphenyl)iminobenzyl-κN,N')pyridine-κN]CoCl2

Base Information

Chemical Name:[bis(N-(2,6-diisopropylphenyl)iminobenzyl-κN,N')pyridine-κN]CoCl2
CAS No.:301658-96-8
Molecular Formula:C₄₃H₄₇Cl₂CoN₃
Molecular Weight:735.765
Hs Code.:

Synonyms:[bis(N-(2,6-diisopropylphenyl)iminobenzyl-κN,N')pyridine-κN]CoCl2

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Chemical Property of [bis(N-(2,6-diisopropylphenyl)iminobenzyl-κN,N')pyridine-κN]CoCl2

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Technology Process of [bis(N-(2,6-diisopropylphenyl)iminobenzyl-κN,N')pyridine-κN]CoCl2

There total 2 articles about [bis(N-(2,6-diisopropylphenyl)iminobenzyl-κN,N')pyridine-κN]CoCl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: bis(2,6-diisopropylphenyliminobenzyl)pyridine

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 301658-96-8
[bis(N-(2,6-diisopropylphenyl)iminobenzyl-κN,N')pyridine-κN]CoCl2

Guidance literature:: In butan-1-ol; Schlenk flasks contg. CoCl2/n-BuOH and ligand/n-BuOH heated to 80°C for 15 min, the Co salt soln. transferred under Ar to the suspn. of ligand, cooled to room temp. during 15 min, stirred for 12 h; concd., pptd. (pentane), filtered, dried (vac.);
DOI:10.1021/ja052129k

Reference yield: 72.0%

: 301658-93-5
2,6-bis[1-[(2,6-di(iso-propyl)phenyl)imino]-benzyl]pyridine

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 301658-96-8
[(2,6-diisopropylphenyl)NC₆H₅]2C₅H₃N cobalt(II) dichloride

Guidance literature:: In butan-1-ol; ligand treated with CoCl2 in n-butanol at 80°C;
DOI:10.1039/b401122h

Reference yield: 74.0%

: 301658-96-8
[bis(N-(2,6-diisopropylphenyl)iminobenzyl-κN,N')pyridine-κN]CoCl2

: 717913-20-7
(2,6-(2,6-ⁱPr₂-C₆H₃-N=CMe)2C₅H₃N)CoCl

Guidance literature:: With CH₃Li; In diethyl ether; toluene; (Ar); a suspn. of Co complex in toluene cooled to -78°C, a soln. of CH3Li in Et2O added dropwise, allowed to warm to room temp. and stirred for 12 h; evapd. (vac.), dissolved in toluene, filtered under Ar through deactivated silica gel, evapd. (vac.), recrystd. at -30°C from toluene;
DOI:10.1021/ja052129k