Technology Process of (Z)-isopropyl 3-(3-(3-cyano-5-isopropoxyphenyl)-1H-1,2,4-triazol-1-yl)acrylate
There total 6 articles about (Z)-isopropyl 3-(3-(3-cyano-5-isopropoxyphenyl)-1H-1,2,4-triazol-1-yl)acrylate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
at 20 ℃;
photo chemical radiation;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate / 20 °C
1.2: 5 h / 80 - 90 °C
2.1: tetrakis / N,N-dimethyl-formamide / 5 h / 80 - 90 °C
3.1: sodium hydrogen sulfide; magnesium chloride / 0.33 h / 20 °C
4.1: diethyl ether / 15 h / 20 °C
5.1: N,N-dimethyl-formamide / 5 h / 20 - 90 °C
6.1: triethylamine / 20 °C / photo chemical radiation
With
sodium hydrogen sulfide; potassium carbonate; triethylamine; magnesium chloride;
tetrakis;
In
diethyl ether; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrakis / N,N-dimethyl-formamide / 5 h / 80 - 90 °C
2: sodium hydrogen sulfide; magnesium chloride / 0.33 h / 20 °C
3: diethyl ether / 15 h / 20 °C
4: N,N-dimethyl-formamide / 5 h / 20 - 90 °C
5: triethylamine / 20 °C / photo chemical radiation
With
sodium hydrogen sulfide; triethylamine; magnesium chloride;
tetrakis;
In
diethyl ether; N,N-dimethyl-formamide;
