tert-butyl 2-azido-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)-phenyl)-3-hydroxypropionate

Base Information

Chemical Name:tert-butyl 2-azido-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)-phenyl)-3-hydroxypropionate
CAS No.:1033617-44-5
Molecular Formula:C₂₂H₃₃N₃O₇S
Molecular Weight:483.586
Hs Code.:

Synonyms:tert-butyl 2-azido-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)-phenyl)-3-hydroxypropionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 2-azido-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)-phenyl)-3-hydroxypropionate

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Technology Process of tert-butyl 2-azido-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)-phenyl)-3-hydroxypropionate

There total 1 articles about tert-butyl 2-azido-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)-phenyl)-3-hydroxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1033617-43-4
tert-butyl 3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)-phenyl)-3-hydroxy-2-(p-nitrobenzenesulfonyl)propionate

: 1033617-44-5
tert-butyl 2-azido-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)-phenyl)-3-hydroxypropionate

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 60 ℃; for 15h;
DOI:10.1016/j.bmc.2008.02.035

Reference yield:

: 1033617-44-5
tert-butyl 2-azido-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)-phenyl)-3-hydroxypropionate

: 1033617-45-6
tert-butyl 2-azido-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)phenyl)-3-fluoropropionate

Guidance literature:: With 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1016/j.bmc.2008.02.035