(2-(S)-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propoxymethyl)benzene

Base Information

• Chemical Name: (2-(S)-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propoxymethyl)benzene
• CAS No.: 885620-02-0
• Molecular Formula: C₁₇H₂₈O₅
• Molecular Weight: 312.406
• Mol file: 885620-02-0.mol

Synonyms:(2-(S)-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propoxymethyl)benzene

Chemical Property of (2-(S)-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propoxymethyl)benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2-(S)-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propoxymethyl)benzene

There total 1 articles about (2-(S)-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propoxymethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate (62921-74-8,518012-62-9,58320-73-3) + (2S)-1-(benzyloxy)propan-2-ol (13807-91-5,89401-28-5,103129-25-5,85483-97-2) → (2-(S)-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propoxymethyl)benzene (885620-02-0)

Guidance literature:

With potassium hydroxide; In tetrahydrofuran; for 24h; Heating;

DOI:10.1021/ja0607234

Reference yield:

(2-(S)-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propoxymethyl)benzene (885620-02-0) → [2-(2-(S)-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propoxy)ethoxymethyl]benzene (889443-57-6)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl; hydrogen / Pd/C / ethanol / 4 h / 20685.9 Torr

2: 55 percent / KOH / tetrahydrofuran / 24 h / Heating

With hydrogenchloride; potassium hydroxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol;

DOI:10.1021/ja0607234

Reference yield:

(2-(S)-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propoxymethyl)benzene (885620-02-0) → 2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-(S)-2-methylethanol (885620-03-1)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; for 4h; under 20685.9 Torr;

DOI:10.1021/ja0607234

upstream raw materials:

2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate

(2S)-1-(benzyloxy)propan-2-ol

Downstream raw materials:

2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-(S)-2-methylethanol

[2-(2-(S)-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propoxy)ethoxymethyl]benzene