(1S,3R,4S,5S)-5-(tert-butyldimethylsilyloxy)-4-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-4-methyl-2-methylenecyclohexanol

Base Information

Chemical Name:(1S,3R,4S,5S)-5-(tert-butyldimethylsilyloxy)-4-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-4-methyl-2-methylenecyclohexanol
CAS No.:1039740-30-1
Molecular Formula:C₂₇H₄₆O₆Si
Molecular Weight:494.744
Hs Code.:

Synonyms:(1S,3R,4S,5S)-5-(tert-butyldimethylsilyloxy)-4-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-4-methyl-2-methylenecyclohexanol

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Chemical Property of (1S,3R,4S,5S)-5-(tert-butyldimethylsilyloxy)-4-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-4-methyl-2-methylenecyclohexanol

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Technology Process of (1S,3R,4S,5S)-5-(tert-butyldimethylsilyloxy)-4-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-4-methyl-2-methylenecyclohexanol

There total 1 articles about (1S,3R,4S,5S)-5-(tert-butyldimethylsilyloxy)-4-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-4-methyl-2-methylenecyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1039740-28-7
tert-butyl[(1S,2S,3R)-2-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-2-methyl-4-methylenecyclohexyloxy]dimethylsilane

: 1039740-30-1
(1S,3R,4S,5S)-5-(tert-butyldimethylsilyloxy)-4-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-4-methyl-2-methylenecyclohexanol

Guidance literature:: With tert.-butylhydroperoxide; selenium(IV) oxide; salicylic acid; In dichloromethane; water; at 20 ℃; for 4h;
DOI:10.1021/jo800913x

Reference yield: 80.0%

: 1039740-30-1
(1S,3R,4S,5S)-5-(tert-butyldimethylsilyloxy)-4-(2,2-dimethoxyethyl)-3-((4-methoxybenzyloxy)methyl)-4-methyl-2-methylenecyclohexanol

: 1039740-32-3
(1S,2S,4S,5S,6R)-4-(tert-butyldimethylsilyloxy)-5-(2,2-dimethoxyethyl)-1-hydroxymethyl-6-((4-methoxybenzyloxy)methyl)-5-methylcyclohexane-1,2-diol

Guidance literature:: With Quinuclidine; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; tert-butyl alcohol; at 20 ℃; for 12h;
DOI:10.1021/jo800913x