C₂₃H₂₇N₅O₅

Base Information

• Chemical Name: C₂₃H₂₇N₅O₅
• CAS No.: 1187660-31-6
• Molecular Formula: C₂₃H₂₇N₅O₅
• Molecular Weight: 453.498
• Mol file: 1187660-31-6.mol

Synonyms:C₂₃H₂₇N₅O₅

Chemical Property of C₂₃H₂₇N₅O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₂₇N₅O₅

There total 8 articles about C₂₃H₂₇N₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C36H51N5O7 (1187660-74-7) → C23H27N5O5 (1187660-31-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 20h;

Reference yield:

C14H20N2O6 (1187660-28-1) → C23H27N5O5 (1187660-31-6)

Guidance literature:

Multi-step reaction with 5 steps

1: hydrogen / palladium on activated charcoal / tetrahydrofuran; thiophene; di-isopropyl ether / 20 h / 20 °C

2: toluene-4-sulfonic acid / 1,4-dioxane / 20 h / 100 °C

3: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C

4: N-ethyl-N,N-diisopropylamine / acetonitrile / 72 h / 70 °C

5: trifluoroacetic acid / dichloromethane / 20 h / 20 °C

With hydrogen; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; thiophene; dichloromethane; di-isopropyl ether; acetonitrile;

Reference yield:

C17H14N2O6 (1187660-26-9) → C23H27N5O5 (1187660-31-6)

Guidance literature:

Multi-step reaction with 7 steps

1: hydrazine hydrate / ethanol / 1 h / 50 °C

2: triethylamine / 1,4-dioxane / 20 °C

3: hydrogen / palladium on activated charcoal / tetrahydrofuran; thiophene; di-isopropyl ether / 20 h / 20 °C

4: toluene-4-sulfonic acid / 1,4-dioxane / 20 h / 100 °C

5: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C

6: N-ethyl-N,N-diisopropylamine / acetonitrile / 72 h / 70 °C

7: trifluoroacetic acid / dichloromethane / 20 h / 20 °C

With hydrogen; toluene-4-sulfonic acid; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; thiophene; ethanol; dichloromethane; di-isopropyl ether; acetonitrile;

upstream raw materials:

C₃₆H₅₁N₅O₇

C₉H₁₂N₂O₄

C₁₄H₂₂N₂O₄

C₁₄H₂₀N₂O₆