(3S,6R)-6-Benzyloxy-2,5-dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine

Base Information

Chemical Name:(3S,6R)-6-Benzyloxy-2,5-dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine
CAS No.:84907-80-2
Molecular Formula:C₂₄H₃₀N₂O₅
Molecular Weight:426.513
Hs Code.:

Synonyms:(3S,6R)-6-Benzyloxy-2,5-dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,6R)-6-Benzyloxy-2,5-dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine

Chemical Property:

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Technology Process of (3S,6R)-6-Benzyloxy-2,5-dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine

There total 2 articles about (3S,6R)-6-Benzyloxy-2,5-dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 79448-86-5
(3S)-2,5-Dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine

: 84907-80-2
(3S,6R)-6-Benzyloxy-2,5-dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine

: 84907-80-2
(3S,6S)-6-Benzyloxy-2,5-dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, hexane, - 70 deg C, 2.) - 70 deg C, 12 h;
DOI:10.1055/s-1982-29979

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 79448-86-5
(3S)-2,5-Dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine

: 84907-80-2
(3S,6R)-6-Benzyloxy-2,5-dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine

: 84907-80-2
(3S,6S)-6-Benzyloxy-2,5-dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, hexane, - 70 deg C, 2.) - 70 deg C, 12 h;
DOI:10.1055/s-1982-29979

Reference yield:

: 84907-80-2
(3S,6R)-6-Benzyloxy-2,5-dimethoxy-3-(3,4-dimethoxybenzyl)-3-methyl-3,6-dihydropyrazine

: 10433-52-0,32520-12-0
O-benzyl-D-serine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 0.1 N aq. HCl, 2.) 25percent aq. NH₃ / 1.) room temp., 4 days

2: 2N aq. HCl / 1 h / Heating

3: methyloxirane / ethanol / 0.25 h / Heating

With hydrogenchloride; ammonium hydroxide; methyloxirane; In ethanol;
DOI:10.1055/s-1982-29979