methyl (R/S)-2-({[4-(4-fluoro-2-thien-3-ylphenoxy)piperidin-1-yl]sulphonyl}methyl)-4-methylpentanoate

Base Information

Chemical Name:methyl (R/S)-2-({[4-(4-fluoro-2-thien-3-ylphenoxy)piperidin-1-yl]sulphonyl}methyl)-4-methylpentanoate
CAS No.:647014-43-5
Molecular Formula:C₂₃H₃₀FNO₅S₂
Molecular Weight:483.625
Hs Code.:

Synonyms:methyl (R/S)-2-({[4-(4-fluoro-2-thien-3-ylphenoxy)piperidin-1-yl]sulphonyl}methyl)-4-methylpentanoate

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Chemical Property of methyl (R/S)-2-({[4-(4-fluoro-2-thien-3-ylphenoxy)piperidin-1-yl]sulphonyl}methyl)-4-methylpentanoate

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Technology Process of methyl (R/S)-2-({[4-(4-fluoro-2-thien-3-ylphenoxy)piperidin-1-yl]sulphonyl}methyl)-4-methylpentanoate

There total 1 articles about methyl (R/S)-2-({[4-(4-fluoro-2-thien-3-ylphenoxy)piperidin-1-yl]sulphonyl}methyl)-4-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6165-69-1
Thien-3-ylboronic acid

: 647014-48-0
methyl (R/S)-2-({[4-(2-bromo-4-fluorophenoxy)piperidin-1-yl]sulphonyl}methyl)-4-methylpentanoate

: 647014-43-5
methyl (R/S)-2-({[4-(4-fluoro-2-thien-3-ylphenoxy)piperidin-1-yl]sulphonyl}methyl)-4-methylpentanoate

Guidance literature:: With sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 85 ℃; for 18h;

Reference yield:

: 647014-43-5
methyl (R/S)-2-({[4-(4-fluoro-2-thien-3-ylphenoxy)piperidin-1-yl]sulphonyl}methyl)-4-methylpentanoate

: (R/S)-2-({[4-(4-fluoro-2-thien-3-ylphenoxy)piperidin-1-yl]sulphonyl}methyl)-N-hydroxy-4-methylpentanamide

Guidance literature:: With hydroxylamine hydrochloride; trimethylaluminum; In toluene; at 5 - 20 ℃; for 1.5h;

methyl (R/S)-2-({[4-(4-fluoro-2-thien-3-ylphenoxy)piperidin-1-yl]sulphonyl}methyl)-4-methylpentanoate; In toluene; at 20 ℃; for 1h;