m-methoxybenzyloxynaphthalenone

Base Information

Chemical Name:m-methoxybenzyloxynaphthalenone
CAS No.:66361-73-7
Molecular Formula:C₁₈H₁₈O₃
Molecular Weight:282.339
Hs Code.:

Synonyms:m-methoxybenzyloxynaphthalenone

Suppliers and Price of m-methoxybenzyloxynaphthalenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of m-methoxybenzyloxynaphthalenone

Chemical Property:

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Technology Process of m-methoxybenzyloxynaphthalenone

There total 1 articles about m-methoxybenzyloxynaphthalenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3470-50-6
6-Hydroxy-1-tetralone

: 824-98-6
m-methoxybenzyl chloride

: 66361-73-7
m-methoxybenzyloxynaphthalenone

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 3h;
DOI:10.1248/cpb.31.2329

Reference yield: 96.0%

: 66361-73-7
m-methoxybenzyloxynaphthalenone

: 66361-74-8
6-(3-Methoxy-benzyloxy)-3,4-dihydro-2H-naphthalen-1-one oxime

Guidance literature:: With hydroxylamine hydrochloride; potassium carbonate; In methanol; water; for 3h; Heating;
DOI:10.1248/cpb.31.2329

Reference yield:

: 66361-73-7
m-methoxybenzyloxynaphthalenone

: 66362-05-8
C₂₅H₂₅NO₅S

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / K₂CO₃/NH₂OH*HCl / methanol; H₂O / 3 h / Heating

2: 95 percent / pyridine / 5 deg C, 30 min, then rt., 1 h

With pyridine; hydroxylamine hydrochloride; potassium carbonate; In methanol; water;
DOI:10.1248/cpb.31.2329