bis[methyl 4-(4-(decyloxy)-2-hydroxybenzylideneamino)benzoato]nickel(II)

Base Information

• Chemical Name: bis[methyl 4-(4-(decyloxy)-2-hydroxybenzylideneamino)benzoato]nickel(II)
• CAS No.: 1613032-45-3
• Molecular Formula: C₅₀H₆₄N₂NiO₈
• Molecular Weight: 879.757
• Mol file: 1613032-45-3.mol

Synonyms:bis[methyl 4-(4-(decyloxy)-2-hydroxybenzylideneamino)benzoato]nickel(II)

Chemical Property of bis[methyl 4-(4-(decyloxy)-2-hydroxybenzylideneamino)benzoato]nickel(II)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis[methyl 4-(4-(decyloxy)-2-hydroxybenzylideneamino)benzoato]nickel(II)

There total 3 articles about bis[methyl 4-(4-(decyloxy)-2-hydroxybenzylideneamino)benzoato]nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

methyl 4-(4'-(decyloxy)-2-hydroxybenzylideneamino)benzoate + nickel diacetate (373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6) → bis[methyl 4-(4-(decyloxy)-2-hydroxybenzylideneamino)benzoato]nickel(II) (1613032-45-3)

Guidance literature:

In methanol; chloroform; at 20 ℃; for 2h;

DOI:10.1080/15421406.2013.803872

Reference yield:

2,4-Dihydroxybenzaldehyde (95-01-2) → bis[methyl 4-(4-(decyloxy)-2-hydroxybenzylideneamino)benzoato]nickel(II) (1613032-45-3)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium iodide; potassium hydrogencarbonate / butanone / 30 h / Reflux

2: acetic acid / ethanol / 4 h / Reflux

3: methanol; chloroform / 2 h / 20 °C

With potassium hydrogencarbonate; acetic acid; potassium iodide; In methanol; ethanol; chloroform; butanone;

DOI:10.1080/15421406.2013.803872

Reference yield:

1-bromo dodecane (112-29-8) → bis[methyl 4-(4-(decyloxy)-2-hydroxybenzylideneamino)benzoato]nickel(II) (1613032-45-3)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium iodide; potassium hydrogencarbonate / butanone / 30 h / Reflux

2: acetic acid / ethanol / 4 h / Reflux

3: methanol; chloroform / 2 h / 20 °C

With potassium hydrogencarbonate; acetic acid; potassium iodide; In methanol; ethanol; chloroform; butanone;

DOI:10.1080/15421406.2013.803872

upstream raw materials:

nickel diacetate

2,4-Dihydroxybenzaldehyde

1-bromo dodecane