9-nitro-4-(4-(trifluoromethyl)benzyl)-3,4,5,6-tetrahydro-2H-imidazo[2,1-b][1,3,6]oxadiazocine

Base Information

Chemical Name:9-nitro-4-(4-(trifluoromethyl)benzyl)-3,4,5,6-tetrahydro-2H-imidazo[2,1-b][1,3,6]oxadiazocine
CAS No.:1437110-45-6
Molecular Formula:C₁₅H₁₅F₃N₄O₃
Molecular Weight:356.304
Hs Code.:

Synonyms:9-nitro-4-(4-(trifluoromethyl)benzyl)-3,4,5,6-tetrahydro-2H-imidazo[2,1-b][1,3,6]oxadiazocine

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Chemical Property of 9-nitro-4-(4-(trifluoromethyl)benzyl)-3,4,5,6-tetrahydro-2H-imidazo[2,1-b][1,3,6]oxadiazocine

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Technology Process of 9-nitro-4-(4-(trifluoromethyl)benzyl)-3,4,5,6-tetrahydro-2H-imidazo[2,1-b][1,3,6]oxadiazocine

There total 2 articles about 9-nitro-4-(4-(trifluoromethyl)benzyl)-3,4,5,6-tetrahydro-2H-imidazo[2,1-b][1,3,6]oxadiazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1437126-63-0
2-((tert-butyldimethylsilyl)oxy)-N-(2-(2,4-dinitro-1H-imidazol-1-yl)ethyl)-N-(4-(trifluoromethyl)benzyl)ethanamine

: 1437110-45-6
9-nitro-4-(4-(trifluoromethyl)benzyl)-3,4,5,6-tetrahydro-2H-imidazo[2,1-b][1,3,6]oxadiazocine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;

Reference yield:

: 1437124-95-2
2-((2-((tert-butyldimethylsilyl)oxy)ethyl)(4-(trifluoromethyl)benzyl)amino)ethanol

: 1437110-45-6
9-nitro-4-(4-(trifluoromethyl)benzyl)-3,4,5,6-tetrahydro-2H-imidazo[2,1-b][1,3,6]oxadiazocine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.58 h / 0 - 20 °C / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; triphenylphosphine; In tetrahydrofuran;