4,5,7-tri-O-benzyl-1,3-dideoxy-1,3-difluoro-α-D-gluco-hept-2-ulopyranose

Base Information

Chemical Name:4,5,7-tri-O-benzyl-1,3-dideoxy-1,3-difluoro-α-D-gluco-hept-2-ulopyranose
CAS No.:1356391-60-0
Molecular Formula:C₂₈H₃₀F₂O₅
Molecular Weight:484.54
Hs Code.:

Synonyms:4,5,7-tri-O-benzyl-1,3-dideoxy-1,3-difluoro-α-D-gluco-hept-2-ulopyranose

Suppliers and Price of 4,5,7-tri-O-benzyl-1,3-dideoxy-1,3-difluoro-α-D-gluco-hept-2-ulopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,5,7-tri-O-benzyl-1,3-dideoxy-1,3-difluoro-α-D-gluco-hept-2-ulopyranose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,5,7-tri-O-benzyl-1,3-dideoxy-1,3-difluoro-α-D-gluco-hept-2-ulopyranose

There total 3 articles about 4,5,7-tri-O-benzyl-1,3-dideoxy-1,3-difluoro-α-D-gluco-hept-2-ulopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1356391-55-3
2,6-anhydro-4,5,7-tri-O-benzyl-1,3-dideoxy-3-fluoro-D-gluco-hept-1-enitol

: 1356391-60-0
4,5,7-tri-O-benzyl-1,3-dideoxy-1,3-difluoro-α-D-gluco-hept-2-ulopyranose

Guidance literature:: With water; Selectfluor; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1055/s-0031-1289598

Reference yield:

: 2-deoxy-2-fluoro-3,4,6-tri-O-benzyl-α,β-D-glucopyranose

: 1356391-60-0
4,5,7-tri-O-benzyl-1,3-dideoxy-1,3-difluoro-α-D-gluco-hept-2-ulopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride; dimethyl sulfoxide / 24 h / 30 °C

2: toluene / 48 h / 75 °C / Inert atmosphere

3: water; Selectfluor / N,N-dimethyl-formamide / 12 h / 20 °C

With water; acetic anhydride; dimethyl sulfoxide; Selectfluor; In N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-0031-1289598

Reference yield:

: 1356391-52-0
3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-D-glucono-1,5-lactone

: 1356391-60-0
4,5,7-tri-O-benzyl-1,3-dideoxy-1,3-difluoro-α-D-gluco-hept-2-ulopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 48 h / 75 °C / Inert atmosphere

2: water; Selectfluor / N,N-dimethyl-formamide / 12 h / 20 °C

With water; Selectfluor; In N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-0031-1289598