N-(2-Trityl-thioethyl)-6-phenyl-4,5-dithiahexanamid

Base Information

• Chemical Name: N-(2-Trityl-thioethyl)-6-phenyl-4,5-dithiahexanamid
• CAS No.: 3312-98-9
• Molecular Formula: C₃₁H₃₁NOS₃
• Molecular Weight: 529.791
• Mol file: 3312-98-9.mol

Synonyms:N-(2-Trityl-thioethyl)-6-phenyl-4,5-dithiahexanamid

Chemical Property of N-(2-Trityl-thioethyl)-6-phenyl-4,5-dithiahexanamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N-(2-Trityl-thioethyl)-6-phenyl-4,5-dithiahexanamid

There total 2 articles about N-(2-Trityl-thioethyl)-6-phenyl-4,5-dithiahexanamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triphenylmethanethiol (3695-77-0) → N-(2-Trityl-thioethyl)-6-phenyl-4,5-dithiahexanamid (3312-98-9)

Guidance literature:

Multi-step reaction with 2 steps

2: DCC / CH₂Cl₂

With dicyclohexyl-carbodiimide; In dichloromethane;

DOI:10.1021/ja01095a032

Reference yield:

2-amino tritylthio ethane (1095-85-8) + 6-Phenyl-4,5-dithia-hexansaeure (3312-95-6) → N-(2-Trityl-thioethyl)-6-phenyl-4,5-dithiahexanamid (3312-98-9)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane;

DOI:10.1021/ja01095a032

Reference yield:

N-(2-Trityl-thioethyl)-6-phenyl-4,5-dithiahexanamid (3312-98-9) → N-(3-Thia-propyl)-6-phenyl-4,5-dithia-hexanamid-disulfid (3313-00-6)

Guidance literature:

With thiocyanogen; boron trifluoride diethyl etherate;

DOI:10.1021/ja01095a032

upstream raw materials:

2-amino tritylthio ethane

6-Phenyl-4,5-dithia-hexansaeure

triphenylmethanethiol

Downstream raw materials:

N-(3-Thia-propyl)-6-phenyl-4,5-dithia-hexanamid-disulfid