Technology Process of C33H35N3O5
There total 11 articles about C33H35N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C
2: sodium hydrogencarbonate / dichloromethane; water / 2 h / 20 °C
3: methanol; isopropyl alcohol / Resolution of racemate
With
hydrogen; sodium hydrogencarbonate;
palladium 10% on activated carbon;
In
methanol; dichloromethane; water; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride; formic acid; water / toluene-4-sulfonic acid / 6 h / Heating / reflux
2: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 1 - 1.5 h / Heating / reflux
3: sodium hydrogencarbonate / dichloromethane; water / 2 h / 20 °C
4: methanol; isopropyl alcohol / Resolution of racemate
With
hydrogenchloride; formic acid; thionyl chloride; water; sodium hydrogencarbonate;
toluene-4-sulfonic acid; N,N-dimethyl-formamide;
In
methanol; dichloromethane; water; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 1 - 1.5 h / Heating / reflux
2: sodium hydrogencarbonate / dichloromethane; water / 2 h / 20 °C
3: methanol; isopropyl alcohol / Resolution of racemate
With
thionyl chloride; sodium hydrogencarbonate;
N,N-dimethyl-formamide;
In
methanol; dichloromethane; water; isopropyl alcohol;