N-[1-Phenyl-1-[2,3,5-trichloro-4-oxo-cyclohexa-2,5-dien-(E)-ylideneamino]-meth-(E)-ylidene]-benzenesulfonamide

Base Information

• Chemical Name: N-[1-Phenyl-1-[2,3,5-trichloro-4-oxo-cyclohexa-2,5-dien-(E)-ylideneamino]-meth-(E)-ylidene]-benzenesulfonamide
• CAS No.: 307553-62-4
• Molecular Formula: C₁₉H₁₁Cl₃N₂O₃S
• Molecular Weight: 453.733

Synonyms:N-[1-Phenyl-1-[2,3,5-trichloro-4-oxo-cyclohexa-2,5-dien-(E)-ylideneamino]-meth-(E)-ylidene]-benzenesulfonamide

Chemical Property of N-[1-Phenyl-1-[2,3,5-trichloro-4-oxo-cyclohexa-2,5-dien-(E)-ylideneamino]-meth-(E)-ylidene]-benzenesulfonamide

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Technology Process of N-[1-Phenyl-1-[2,3,5-trichloro-4-oxo-cyclohexa-2,5-dien-(E)-ylideneamino]-meth-(E)-ylidene]-benzenesulfonamide

There total 4 articles about N-[1-Phenyl-1-[2,3,5-trichloro-4-oxo-cyclohexa-2,5-dien-(E)-ylideneamino]-meth-(E)-ylidene]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N-[1-Phenyl-1-(2,3,5-trichloro-4-hydroxy-phenylamino)-meth-(Z)-ylidene]-benzenesulfonamide (307553-65-7) → N-[1-Phenyl-1-[2,3,5-trichloro-4-oxo-cyclohexa-2,5-dien-(E)-ylideneamino]-meth-(E)-ylidene]-benzenesulfonamide (307553-62-4)

Guidance literature:

With chlorine; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1023/A:1016555324390

Reference yield: 73.0%

N2-Benzolsulfonyl-N1-(4'-hydroxyphenyl)benzamidin (31789-77-2) → N-[1-Phenyl-1-[2,3,5-trichloro-4-oxo-cyclohexa-2,5-dien-(E)-ylideneamino]-meth-(E)-ylidene]-benzenesulfonamide (307553-62-4)

Guidance literature:

With chlorine; In N,N-dimethyl-formamide; at 30 ℃;

DOI:10.1023/A:1016555324390

Reference yield:

N-(N-phenylsulfonylbenzimidoyl)-1,4-benzoquinone imine (494210-55-8) → N-[1-Phenyl-1-[2,3,5-trichloro-4-oxo-cyclohexa-2,5-dien-(E)-ylideneamino]-meth-(E)-ylidene]-benzenesulfonamide (307553-62-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 83 percent / Cl₂ / acetic acid; dimethylformamide / 20 °C

2: 96 percent / Cl₂ / dimethylformamide / 20 °C

With chlorine; In acetic acid; N,N-dimethyl-formamide;

DOI:10.1023/A:1016555324390

upstream raw materials:

N²-Benzolsulfonyl-N¹-(4'-hydroxyphenyl)benzamidin

N-[1-Phenyl-1-(2,3,5-trichloro-4-hydroxy-phenylamino)-meth-(Z)-ylidene]-benzenesulfonamide

N-(N-phenylsulfonylbenzimidoyl)-1,4-benzoquinone imine

N-(N-phenylsulfonylbenzimidoyl)-2-chloro-1,4-benzoquinone imine

Downstream raw materials:

N-[1-Phenyl-1-(2,3,5,6-tetrachloro-4-oxo-cyclohexa-2,5-dienylideneamino)-meth-(Z)-ylidene]-benzenesulfonamide

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