(S)-5-benzoyloxy-2-methylcyclohex-1-ene-1-carbaldehyde

Base Information

Chemical Name:(S)-5-benzoyloxy-2-methylcyclohex-1-ene-1-carbaldehyde
CAS No.:75212-00-9
Molecular Formula:C₁₅H₁₆O₃
Molecular Weight:244.29
Hs Code.:

Synonyms:(S)-5-benzoyloxy-2-methylcyclohex-1-ene-1-carbaldehyde

Suppliers and Price of (S)-5-benzoyloxy-2-methylcyclohex-1-ene-1-carbaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-5-benzoyloxy-2-methylcyclohex-1-ene-1-carbaldehyde

Chemical Property:

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Technology Process of (S)-5-benzoyloxy-2-methylcyclohex-1-ene-1-carbaldehyde

There total 7 articles about (S)-5-benzoyloxy-2-methylcyclohex-1-ene-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 8a-methyl-6-β-hydroxy-3,5,6,7,8,8a-hexahydro-1-benzopyran-2-one

: 75212-00-9
(S)-5-benzoyloxy-2-methylcyclohex-1-ene-1-carbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 89.2 percent / pyridine / 2 h / Ambient temperature

2: 1.) sodium hydride, 2.) trifluoroacetic acid / benzene / 2 h / Heating

3: benzene

4: osmium tetroxide / pyridine / 2 h / Ambient temperature

5: sodium periodate / acetone / Ambient temperature

With pyridine; sodium periodate; osmium(VIII) oxide; sodium hydride; trifluoroacetic acid; In pyridine; acetone; benzene;

Reference yield:

: 96700-66-2
8a-methyl-3,4,7,8-tetrahydro-1-benzopyran-2,6-dione

: 75212-00-9
(S)-5-benzoyloxy-2-methylcyclohex-1-ene-1-carbaldehyde

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / 40 percent HBr in acetic acdid / Ambient temperature

2: 79.2 percent / NaBH₄ / methanol / 1.5 h / 10 - 20 °C

3: 89.2 percent / pyridine / 2 h / Ambient temperature

4: 1.) sodium hydride, 2.) trifluoroacetic acid / benzene / 2 h / Heating

5: benzene

6: osmium tetroxide / pyridine / 2 h / Ambient temperature

7: sodium periodate / acetone / Ambient temperature

With pyridine; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; hydrogen bromide; sodium hydride; trifluoroacetic acid; In pyridine; methanol; acetone; benzene;

Reference yield:

: 96700-67-3
8a-methyl-6-acetoxy-3,7,8,8a-tetrahydro-1-benzopyran-2-one

: 75212-00-9
(S)-5-benzoyloxy-2-methylcyclohex-1-ene-1-carbaldehyde

Guidance literature:: Multi-step reaction with 6 steps

1: 79.2 percent / NaBH₄ / methanol / 1.5 h / 10 - 20 °C

2: 89.2 percent / pyridine / 2 h / Ambient temperature

3: 1.) sodium hydride, 2.) trifluoroacetic acid / benzene / 2 h / Heating

4: benzene

5: osmium tetroxide / pyridine / 2 h / Ambient temperature

6: sodium periodate / acetone / Ambient temperature

With pyridine; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; sodium hydride; trifluoroacetic acid; In pyridine; methanol; acetone; benzene;